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← Document results/DEP Box 60/GCMS Scan X 10/5/01 An 10/25/01
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GCMS calibration table for TCLP analysis, Oct 25 2001

Machine-extracted title · confidence 95%

Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.

NYC-WTC_000067739–000067751

Folder label: “GCMS Scan X 10/5/01 An 10/25/01”

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NYC 9/11 Public Portal Document / Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\l\data\oct2501\LB.D Vial: 2 Acq On : 25 Oct 2001 11:58 am Operator: 209 GALOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 25 12:46 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 3 8) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 20.63 165 166408 4.93 ug/1 # 44 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 21.08 165 179 N.D. 45) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 25.07 178 548 N.D. 5 6) Anthracene 25.07 178 548 N.D. 57) Di-n-butylphthalate 27.06 149 2922 N.D. 5 8) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 0.00 184 0 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 33.10 228 2756 N.D. 66) Bis(2-ethylhexyl)phthalate 33.36 149 4659 N.D. 67) Chrysene 33.10 228 2756 N.D. 69) Di-n-Octylphthalate 0.00 149 0 N.D. 70) Benzo(b)fluoranthene 0.00 252 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP101901.M Thu Oct 25 12:47:08 2001 Page 2

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