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← Document results/DEP Box 60/GCMS Scan X 10/5/01 An 10/25/01
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GCMS calibration table for TCLP analysis, Oct 25 2001

Machine-extracted title · confidence 95%

Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.

NYC-WTC_000067739–000067751

Folder label: “GCMS Scan X 10/5/01 An 10/25/01”

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\l\data\oct2501\LB.D^ Vial: 2 Acq On : 25 Oct 2001 11:58 am ® Operator: 209 GALOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 25 12:46 2001 ' Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.74 152 632521 20.00 ug/1 -0.02 19) Naphthalene-d8 15.35 136 2597946 20.00 ug/1 -0.02 31) Acenaphthene-dlO 20.63 164 1287352 20.00 ug/1 0.00 49) Phenanthrene-dlO 25.06 188 1925321 20.00 ug/1 0.00 59) Chrysene-dl2 33.09 240 1071271 20.00 ug/1 0.00 68) Perylene-dl2 37.20 264 738375 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.74 132 314 0.00 ug/1 0.48 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.25 152 6824 0.16 ug/1 -0.02 Spiked Amount 50.000 Recovery = 0.32% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.78 172 2736 0.02 ug/1 0.13 Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP101901.M Thu Oct 25 12:47:03 2001 Page 1

NYC-WTC_000067739

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GCMS sample extraction log table, Nov 2001 · Box DEP Box 60

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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