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GCMS calibration table for TCLP analysis, Oct 25 2001

Machine-extracted title · confidence 95%

Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.

NYC-WTC_000067739–000067751

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\l\data\oct2501\LB.D Vial: 2 Acq On : 25 Oct 2001 11:58 am Operator: 209 GALOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 25 12:46 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Compound R.T. Qlon Response Cone Unit Qvalue 71) Benzo(k)fluoranthene 0.00 252 0 N.D. 72) Benzo(a)pyrene 37.20 252 2853 N.D. 73) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 74) Dibenz(a,h)anthracene 0.00 278 0 N.D. 75) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D NP101901.M Thu Oct 25 12:47:09 2001 Page 3

NYC-WTC_000067741

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NYC-WTC_000067741Source: NYC Law Department, mirrored locally

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GCMS sample extraction log table, Nov 2001 · Box DEP Box 60

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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