GCMS Method 508 sample analysis results, April 9 2002

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Library Search Compound Report

Data.File C:\MSDCHEM\l\DATA\020409\6338.D Vial: 7 Acq On 9 Apr 2002 8:45 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number , 3 Phenanthrene-dlO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.14 0.20 ug/1 229823 Phenanthrene-dl0 30.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 83 3 Naphthalene, 1,7-dimethoxy- 188 C12H12O2 005309-18-2 9 4 Naphthalene, 2,7-dimethoxy- 188 C12H12O2 003469-26-9 9 Abundance Scan 4775 (31.135 min): 6338.D (-4764) (-) m/z 188.10 100.00% 1(8

2551

80 94 30.80 31.00 31.20 31.40 m/z 189.20 17769% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-dlO 1(8

5000 30.80 31.00 31.20 31.40 m/z 94710 15.36% RG 94 160

Tl/Z-> .. . ..... I. ............. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-dlO- 1(8 7 \........................................ y.8O 31.00 31.20 31.40 5000 m/z SOTOO 14732%

„ 80 94 .|eQ ,

■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance! #79804: Naphthalene, 1,7-dimethoxy- 173 1(18 y.8O 31.00 31.20 31.40 m/z 184.10 14.01%

5000

102 145

51 63 75 130 158 I ‘ ' 11" ’ I' ' T" " 1" '' J' 'I I''. 11.. 1111 T~ ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 30.80 31.00 31 20 31.40

6338.D SCANAPR0902.M Thu May 02 14:06:51 2002 Page 5

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