GCMS sample analysis summary, March 2002

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' Data File C:\MSDCHEM\l\DATA\022802\03016.D Vial: 9 Acq On 1 Mar 2002 6:56 pm Operator: McLean Sample 2/12/02 GC SCAN Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 .Phenanthrene-dlO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.68 0.21 ug/L 97016 Phenanthrene-dl0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrerfe-dlO 188 C14D10 001517-22-2 72 2 DECADEUTEIffi PHENANTHRENE $$ Phena. . . 188 C14D10 001517-22-2 72 3 Anthracep^-DlO 188 C14D10 000000-00-0 64 4 1-methylyVS-methoxy- 1,4-epoxynaph. . . 188 C12H12O2 000000-00-0 59 Abundance Scan 2161 (22.677 min): 03016.D (-) m/z 188.15 100.00% 1!8

5000

78 “ 160 22.40 22.60 22.80 23.00 O'I . ■ . ■ I . |l[ , , , , I lll.|. , , , m/z 94.10 1773?% m/z-> 20 40 60__ 80 100 120 140 160 180 200 Abundance #84499; Phenanthrene-dlO 168

5000 T^ 22.40 22.60 22.80 23.00 m/z 189.15 12767% 80 94 160 ,30,42 52 66 0 I ' ' ' ' I ' ' ' ' I ‘ ' I ' I 108118 132 146 170 1 m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #84500: DECADEUTEROPHENANTHRENE $S Phenanthrene-dlO 188

22.40 22.60 22.80 23.00 5000 m/z 78.10 12.07%

80 94 I 30 42 52 66 I 1081,18 132 J,46170 j OS-’ •n/z-> 20 40 60 80 100 120 140 ■ 160 180 200 Abundance #84498; Anthracene-DIO 188 ' ' I ' ’ 22.40 22.60 22.80 23.00 m/z 160.10 11.97%'

5000

94 66 160 0 108118 132 146 4^ 1 m/z-> 20 40 60 80 100 120 140 160 180 200 22.40 22.60 22.80 23.00

)3016.D 032802.M Tue Apr 02 07:01:44 2002 Page 5

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