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GCMS analysis results for sample AE03182, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AE03182 conducted on March 22, 2002.

NYC-WTC_000011177–000011188

Folder label: “GCMS X 2/12/02 A 3/19/02

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Scanned page image, NYC-WTC_000011187
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031802\3182.D Vial: 14 Acq On : 19 Mar 2002 12:49 pm Operator: McLean Sample : GC/MS SCAN 3/6 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 22.64 0.41 ug/L 151943 Phenanthrene -dl0 22.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 64 2 Anthracene-D10 188 C14D10 000000-00-0 53 3 Anthracene-dlO- 188 C14D10 001719-06-8 53 4 Phenanthrene-diO 188 C14D10 001517-22-2 52 Abundance Scan 2157 (22.641 mln): 3182.D (-) m/z 188.15 100.00% 188

5000 76 54 94 158 d/*1/1///21/8/0/0/01/n//0/6//k.n.n 22.40 22.60 22.80 23.00

/z—> OVt 20 40 60 80 i • • 100 120 140 160 180 200 *I*’’*I**’’I* ponoep ‘ • i ‘ m/z 76.10 30.82%

Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-dlO 188

5000 - 22.40 22.60 22.80 23.00 m/z 158.10 26.24% 80 94 40 52 66 , 108 132 146 158 170 It 0+r ■ i ■ 29 • 1 'f11 i 11 1 ' I1 mmt lz-> 20 40 60 80 100 120 140 160 180 200 Abundance #84498: Anthracene-D10 188

’**’I**** 1*’** 1****I8* 22.40 22.60 22.80 23.00 5000 m/z 94.10 22.26%

80 . 94 66 160

mlz-> OtT .39115, 20 40 60 .80I. 198 —1132,146..,, 1 1 1 f ’ 11" 100 120 140 160 180 200 Abundance #84502: Anthracene-d10- 1118 —m mmmpo 22.40 22.60 22.80 23.00 m/z 54.00 22.02%

5000

80 94 160 OTri17। 28rr]40’t ■52r, i'll, 66 , 106118 132 146,11 TI"PI -,-H p-rrrri 11* .. , 7 . /z—> 20 40 60 80 100 120 140 160 180 200 22.40 22.60 22.80 23.00

3182.D 5080302.M Tue Mar 19 21:39:39 2002 Page 3

NYC-WTC_000011187

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NYC-WTC_000011187Source: NYC Law Department, mirrored locally

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