Analysis of reference standards for nitrosamines and VOCs with measured concentrations near target levels on March 29, 2002.
NYC-WTC_000058175–000058182Folder label: “GCMS X 3/2/02 A 3/27/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR2702\REF2.D Vial: 5 Acq On : 27 Mar 2002 5:37 pm Operator: Sample : gc/ms scan 3/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 12:36 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ; Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Confound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.22 168 149273 4.86 ug/1 # 82 31) 4-Bromophenyl-phenylether 24.30 248 104533 5.80 ug/1 # 90 32) Hexachlorobenzene 24.73 284 127185 6.07 ug/1 90 3 3) Phenanthrene 25.70 178 553685 5.64 ug/1 98 34) Anthracene 25.83 178 522876 5.37 ug/1 99 35) Di-n-butylphthalate 27.60 149 798462 6.47 ug/1 99 36) Fluoranthene 29.33 202 536573 5.21 ug/1 96 39) Pyrene 30.01 202 558267 7.88 ug/1 95 40) Butylbenzylphthalate 32.14 149 232872 6.37 ug/1 # 97 41) Benzo(a)anthracene 33.64 228 322503 5.47 ug/1 99 42) Bis{2-ethylhexyl)phthalate 33.91 149 293984 5.96 ug/1 96 43) Chrysene 33.77 228 349307 6.04 ug/1 98 45) Di-n-Octylphthalate 35.65 149 331051 5.51 ug/1 # 97 4 6) Benzo(b)fluoranthene 36.75 252 237877m 5.71 ug/1 47) Benzo(k)fluoranthene 36.82 252 266359 6.56 ug/1 97 48) Benzo(a)pyrene 37.75 252 172510 4.55 ug/1 97 . 49) Indeno(1,2,3-cd)pyrene 42.06 276 156174 3.41 ug/1 96 5 0) Dibenz(a,h)anthracene 42.14 278 130895 3.69 ug/1 98 51) Benzo(g,h,i)perylene 43.30 276 137637 3.68 ug/1 96
(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Fri Mar 29 12:37:25 2002 Page 2
NYC-WTC_000058181
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NYC-WTC_000059118
Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
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Laboratory report showing GCMS calibration analysis for volatile organic compounds on April 2, 2002.
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Laboratory report listing concentrations of target analytes in a reference standard analyzed on March 29, 2002.
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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058911
Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059222
Reference standard analysis report for volatile organic compounds using GCMS on April 4, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058258
Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.
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Calibration data sheet listing retention times and response factors for multiple organic compounds analyzed on April 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011849
Reference analysis record for GCMS testing of sample AE04388 conducted on March 28, 2002, by analyst MG.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037996
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE03823 analyzed on March 26, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011711
Calibration record for GCMS analysis of sample AE04038 conducted on March 27, 2002, showing compound responses.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010289
Reference data report displaying measured concentrations and detection limits for target analytes analyzed on March 21, 2002.
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NYC-WTC_000058159
Unreadable text fragment containing a file identifier from the March 2002 GCMS batch records.
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NYC-WTC_000058160
Fragmented text containing a unique file identifier from the March 2002 GCMS batch records.
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NYC-WTC_000058163
Laboratory blank analysis report showing all target compounds detected below the method detection limit on March 29, 2002.
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NYC-WTC_000058171
Calibration log listing response factors for nitrosamines and chlorinated solvents on March 29, 2002.
Filed in the same folder
NYC-WTC_000058183
GCMS analysis of sample AE04416 for organic compounds with surrogate standard showing 5.0 micrograms detection limit.
Filed in the same folder