Analysis of reference standards for nitrosamines and VOCs with measured concentrations near target levels on March 29, 2002.
NYC-WTC_000058175–000058182Folder label: “GCMS X 3/2/02 A 3/27/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C;\HPCHEM\1\DATA\MAR27O2\REF1.D Vial: 4 Acq On : 27 Mar 2002 4:37 pm Operator : San^le ; gc/ms scan 3/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 12:29 2002 Quant Results Pile: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.22 168 171862 4.94 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.29 248 121360 5.94 ug/1 91 3 2) Hexachlorobenzene 24.73 284 146504 6.17 ug/1 # 87 3 3) Phenanthrene 25.71 178 647230 5.82 ug/1 99 34) Anthracene 25.84 178 618268 5.61 ug/1 99 35) Di-n-butylphthalate 27.61 149 909379 6.50 ug/1 # 98 36) Fluoranthene 29.32 202 626139 5.37 ug/1 # 94 39) Pyrene 30.00 202 648761 8.03 ug/1 # 92 40) Butylbenzylphthalate 32.13 149 275030 6.60 ug/1 98 41) Benzo{a)anthracene 33.65 228 381078 5.67 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.91 149 342875 6.09 ug/1 # 94 43) Chrysene 33.78 228 405715 6.15 ug/1 99 45) Di-n-Octylphthalate 35.65 149 391737 5.61 ug/1 # 98 46) Benzo(b)fluoranthene 36.75 252 292751 6.05 ug/1 97 47) Benzo(k)fluoranthene 36.82 252 321150 6.81 ug/1 97 48) Benzo(a)pyrene 37.74 252 209087 4.74 ug/1 # 97 49) Indeno{l,2,3-cd)pyrene 42.06 276 187918 3.53 ug/1 96 50) Dibenz(a,h)anthracene 42.13 278 160793 3.90 ug/1 98 51) Benzo(g,h,i)perylene 43.30 276 170342 3.92 ug/1 93
(#) = qualifier out of range (m) = manual integration REFl.D GCMS0308.M Fri Mar 29 12:59:31 2002 Page 2
NYC-WTC_000058178
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NYC-WTC_000059118
Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
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Laboratory report showing GCMS calibration analysis for volatile organic compounds on April 2, 2002.
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Laboratory report listing concentrations of target analytes in a reference standard analyzed on March 29, 2002.
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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.
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Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.
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Reference standard analysis report for volatile organic compounds using GCMS on April 4, 2002.
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Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.
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Calibration data sheet listing retention times and response factors for multiple organic compounds analyzed on April 5, 2002.
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Reference analysis record for GCMS testing of sample AE04388 conducted on March 28, 2002, by analyst MG.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037996
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE03823 analyzed on March 26, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011711
Calibration record for GCMS analysis of sample AE04038 conducted on March 27, 2002, showing compound responses.
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Reference data report displaying measured concentrations and detection limits for target analytes analyzed on March 21, 2002.
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NYC-WTC_000058727
Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.
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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.
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Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.
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Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038756
Laboratory report listing quantitative results for volatile organic compounds in sample AE02567 analyzed on March 21, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059687
Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.
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NYC-WTC_000058159
Unreadable text fragment containing a file identifier from the March 2002 GCMS batch records.
Filed in the same folder
NYC-WTC_000058160
Fragmented text containing a unique file identifier from the March 2002 GCMS batch records.
Filed in the same folder
NYC-WTC_000058163
Laboratory blank analysis report showing all target compounds detected below the method detection limit on March 29, 2002.
Filed in the same folder
NYC-WTC_000058171
Calibration log listing response factors for nitrosamines and chlorinated solvents on March 29, 2002.
Filed in the same folder
NYC-WTC_000058183
GCMS analysis of sample AE04416 for organic compounds with surrogate standard showing 5.0 micrograms detection limit.
Filed in the same folder