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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09156 Sample Date/Time: Wednesday, May 08, 2002 11:56:02 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE091 56.793 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 14.667 27.555 0.000 - 0.00900 120.90 ug/L Se-1 45 490559.304 1.665 490559.304 ug/L Cr 52 7641.287 0.930 -0.000 -0.01594 33.37 ug/L Cr 53 2079.925 1.327 0.003 0.97674 3.79 ug/L Mn 55 1823703.192 1.557 3.705 100.90796 3.00 ug/L Ni 60 14516.728 1.611 0.029 5.01167 2.49 ug/L Cu 63 146372.352 1.899 0.298 22.67566 1.39 ug/L Cu 65 73732.893 1.094 0.150 23.24764 0.79 ug/L Zn 66 451226.713 0.521 3.774 227.34740 0.48 ug/L Zn 67 70299.804 0.440 0.587 195.96942 0.45 ug/L Zn 68 337737.984 1.640 2.824 224.02845 1.45 ug/L > Ge 72 119389.034 0.354 119389.034 ug/L As 75 14106.628 1.518 0.028 1.36467 7.22 ug/L Se 77 2073.660 1.094 0.005 2.91680 4.17 ug/L Se 82 732.294 10.709 0.007 2.93708 10.07 ug/L Kr 83 4112.304 0.736 -349.168 ug/L Ag 107 129.336 12.760 -0.000 -0.01738 6.84 ug/L in 115 1727354.503 1.300 1727354.503 ug/L Sb 121 1096.410 2.965 0.001 0.08320 2.94 ug/L Sb 123 837.315 8.806 0.000 0.08191 8.66 ug/L Ba 135 93107.120 2.292 0.036 24.57437 1.90 ug/L Ba 137 165506.250 1.721 0.064 24.94585 1.32 ug/L Tb 159 2580890.874 0.403 2580890.874 ug/L Hg 201 127.336 5.346 0.000 0.00421 92.88 ug/L Hg 202 278.007 0.952 0.000 0.00539 10.80 ug/L TI 205 4916.712 2.545 0.001 0.08460 3.37 ug/L Pb 208 14337.205 1.005 0.004 0.21926 1.75 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 95.932 Cr 52 Cr 53 Mn 55

Sample ID: AE09156 Report Date/Time: Wednesday, May 08, 2002 11:57:43 Page 1

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