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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09765 Sample Date/Time: Tuesday, May 14, 2002 10:24:43 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09765.022 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 9.667 31.604 0.000' 0.00186 337.30 ug/L Se-1 45 597381.025 0.592 597381.025 ug/L Cr 52 12907.953 0.620 0.007 0.30629 3.72 ug/L Cr 53 2712.099 4.902 0.003 1.22041 7.92 ug/L Mn 55 384068.625 1.437 0.641 17.86050 2.03 ug/L Ni 60 1122.080 2.412 0.002 0.34271 3.09 ug/L Cu 63 8752.966 1.207 0.014 1.24779 1.72 ug/L Cu 65 4203.347 1.073 0.007 1.24960 0.52 ug/L Zn 66 6018.385 0.728 0.038 2.24186 1.09 ug/L Zn 67 1152.751 3.286 0.007 2.45164 2.90 ug/L Zn 68 5127.165 4.201 0.033 2.61481 3.80 ug/L Ge 72 130947.041 0.980 130947.041 ug/L As 75 7022.763 0.798 0.009 0.44135 10.47 ug/L Se 77 970.154 0.858 0.001 0.45682 15.63 ug/L Se 82 -10.882 1097.293 0.000 0.01503 2683.12 ug/L Kr 83 2363.331 4.033 -141.373 ug/L Ag 107 136.669 8.851 -0.000 -0.01385 6.17 ug/L > in 115 1717473.006 1.020 1717473.006 ug/L Sb 121 558.356 4.968 0.000 0.04952 4.25 ug/L Sb 123 434.828 6.468 0.000 0.04998 6.02 ug/L Ba 135 56319.826 1.098 0.021 15.94916 0.69 ug/L Ba 137 98926.072 1.541 0.036 15.92905 1.16 ug/L > Tb 159 2742971.209 0.414 2742971.209 ug/L Hg 201 71.001 4.225 0.000 0.01390 13.88 ug/L Hg 202 141.003 9.853 0.000 0.01105 33.56 ug/L n 205 971.728 1.798 -0.000 -0.00013 396.71 ug/L Pb 208 6311.922 1.990 0.001 0.06474 3.01 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 84.771 Cr 52 Cr 53 Mn 55

Sample ID: AE09765 Report Date/Time: Tuesday, May 14, 2002 10:26:24 Page 1

NYC-WTC_000053432

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