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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09446 Sample Date/Time: Wednesday, May 08, 2002 13:20:40 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd 1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09446.807 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Gone. Mean Cone. RSD Sample Unit Be 9 14.000 37.796 0.000 - 0.01019 151.71 ug/L > Se-1 45 456837.546 4.520 456837.546 ug/L Cr 52 7681.656 2.715 0.001 0.04150 96.29 ug/L Cr 53 1486.803 0.272 0.002 0.60380 8.79 ug/L Mn 55 303422.799 1.018 0.651 17.73795 4.36 ug/L Ni 60 1162.753 0.866 0.002 0.40100 5.85 ug/L Cu 63 9027.237 1.532 0.019 1.46768 4.66 ug/L Cu 65 4354.086 1.208 0.009 1.42373 4.45 ug/L Zn 66 7820.442 2.939 0.061 3.69321 4.61 ug/L Zn 67 1430.127 1.696 0.011 3.64949 1.95 ug/L Zn 68 6440.345 1.267 0.050 3.99512 1.03 ug/L > Ge 72 116403.097 1.540 116403.097 ug/L As 75 11556.342 0.429 0.009 0.45371 17.42 ug/L Se 77 1463.024 0.745 0.001 0.36332 21.49 ug/L Se 82 -119.840 41.903 -0.001 -0.23947 82.94 ug/L Kr 83 4116.973 1.639 -344.499 ug/L Ag 107 343.677 4.924 -0.000 -0.00252 39.19 ug/L > In 115 1703528.713 1.266 1703528.713 ug/L Sb 121 651.363 2.580 0.000 0.04631 3.01 ug/L Sb 123 519.900 3.935 0.000 0.04762 3.73 ug/L Ba 135 54305.262 0.706 0.021 14.51994 1.88 ug/L Ba 137 95441.343 0.604 0.037 14.57229 1.47 ug/L Tb 159 2547212.240 1.368 2547212.240 ug/L Hg 201 109.668 10.249 -0.000 -0.00494 142.33 ug/L Hg 202 230.672 7.181 -0.000 -0.00576 59.10 ug/L TI 205 829.380 4.968 -0.000 -0.01849 7.27 ug/L Pb 208 7401.578 1.016 0.002 0.08901 2.44 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 89.337 Cr 52 Cr 53 Mn 55

Sample ID: AE09446 Report Date/Time: Wednesday, May 08, 2002 13:22:21 Page 1

NYC-WTC_000053157

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