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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09766 Sample Date/Time: Tuesday, May 14, 2002 10:48:18 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09766.026 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 8.667 17.625 0.000 ' 0.00013 2504.95 ug/L Se-1 45 587082.271 0.479 587082.271 ug/L Cr 52 10317.288 1.111 0.003 0.11756 9.11 ug/L Cr 53 3899.876 3.838 0.005 2.04904 5.28 ug/L Mn 55 1230561.599 2.063 2.094 58.34817 2.05 ug/L Ni 60 3576.073 2.989 0.006 1.13795 3.21 ug/L Cu 63 72778.920 1.328 0.123 10.91884 1.44 ug/L Cu 65 34716.522 1.751 0.059 10.87969 1.91 ug/L Zn 66 15653.958 1.434 0.115 6.76105 1.01 ug/L Zn 67 2775.118 3.301 0.020 6.79499 3.38 ug/L Zn 68 12760.079 1.952 0.094 7.42062 0.78 ug/L > Ge 72 127638.140 1.220 127638.140 ug/L As 75 6937.631 2.739 0.010 0.47601 8.86 ug/L Se 77 1112.536 2.762 0.002 1.14320 8.40 ug/L Se 82 -0.595 8519.962 0.000 0.04656 378.38 ug/L Kr 83 2292.312 2.766 -212.392 ug/L Ag 107 1426.795 17.527 0.001 0.07652 20.21 ug/L in 115 1663531.967 2.071 1663531.967 ug/L Sb 121 848.048 0.657 0.000 0.07943 1.46 ug/L Sb 123 623.719 2.961 0.000 0.07590 1.00 ug/L Ba 135 99428.816 1.182 0.037 28.54871 0.69 ug/L Ba 137 173541.617 1.144 0.064 28.33253 0.82 ug/L > Tb 159 2706528.800 0.563 2706528.800 ug/L Hg 201 182.337 18.398 0.000 0.08050 24.25 ug/L Hg 202 409.680 20.100 0.000 0.08127 25.69 ug/L TI 205 926.056 1.245 -0.000 -0.00093 31.21 ug/L Pb 208 59274.034 1.307 0.021 1.11525 1.35 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 83.309 Cr 52 Cr 53 Mn 55

Sample ID: AE09766 Report Date/Time: Tuesday, May 14, 2002 10:49:58 Page 1

NYC-WTC_000053440

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