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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09452 Sample Date/Time: Wednesday, May 08, 2002 13:41:42 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09452.813 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 14.667 34.317 0.000 0.01208 110.09 ug/L > Se-1 45 450890.441 2.083 450890.441 ug/L Cr 52 7548.542 1.211 0.001 0.03733 49.54 ug/L Cr 53 1552.815 2.656 0.002 0.67491 8.97 ug/L Mn 55 404395.022 1.535 0.883 24.05811 2.10 ug/L Ni 60 1223.761 4.915 0.003 0.42921 5.82 ug/L Cu 63 59063.168 0.371 0.131 9.93623 2.34 ug/L Cu 65 29405.778 0.957 0.065 10.05756 2.11 ug/L Zn 66 7483.821 1.814 0.059 3.54261 1.99 ug/L Zn 67 1399.455 1.728 0.011 3.58804 3.30 ug/L Zn 68 6170.489 1.155 0.048 3.83858 2.07 ug/L Ge 72 115658.640 1.266 115658.640 ug/L As 75 11768.810 1.593 0.012 0.57362 24.00 ug/L Se 77 1477.126 2.274 0.001 0.47256 51.25 ug/L Se 82 60.840 255.617 0.001 0.45675 132.08 ug/L Kr 83 4009.925 2.224 -451.548 ug/L Ag 107 215.338 5.178 -0.000 -0.01135 8.79 ug/L in 115 1704465.937 1.541 1704465.937 ug/L Sb 121 616.694 7.147 0.000 0.04329 7.82 ug/L Sb 123 473.824 4.834 0.000 0.04246 7.86 ug/L Ba 135 56068.937 0.606 0.022 14.93690 0.95 ug/L Ba 137 97781.396 1.040 0.038 14.87490 0.05 ug/L > Tb 159 2556309.245 1.032 2556309.245 ug/L Hg 201 91.668 16.339 -0.000 -0.01550 56.37 ug/L Hg 202 190.671 8.131 -0.000 -0.01605 26.91 ug/L TI 205 764.707 10.610 -0.000 -0.02024 9.46 ug/L Pb 208 34859.514 0.975 0.013 0.61655 0.32 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff ' Be 9 > Sc-1 45 88.174 Cr 52 Cr 53 Mn 55

Sample ID: AE09452 Report Date/Time: Wednesday, May 08, 2002 13:43:23 Page 1

NYC-WTC_000053169

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