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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09970 Sample Date/Time: Tuesday, May 14, 2002 11:33:19 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd 1 \elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09970.037 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean. Cone. Mean Cone. RSD Sample Unit Be 9 9.000 11.111 0.000 0.00164 112.45 ug/L Se-1 45 561478.820 1.841 561478.820 ug/L Cr 52 11536.100 2.409 0.005 0.25657 5.40 ug/L Cr 53 3010.195 2.364 0.004 1.54358 0.73 ug/L Mn 55 513765.465 1.804 0.913 25.44289 1.59 ug/L Ni 60 1302.440 3.931 0.002 0.42588 2.47 ug/L Cu 63 46039.440 1.921 0.081 7.20607 1.52 ug/L Cu 65 21986.443 1.072 0.039 7.18879 2.25 ug/L Zn 66 4606.213 1.031 0.030 1.74823 2.10 ug/L Zn 67 988.730 3.319 0.007 2.20578 5.24 ug/L Zn 68 4030.600 1.670 0.027 2.12007 1.01 ug/L > Ge 72 122561.245 1.024 122561.245 ug/L As 75 6605.245 1.733 0.009 0.45433 15.62 ug/L Se 77 955.110 1.163 0.001 0.65881 13.17 ug/L Se 82 -37.165 140.250 -0.000 -0.08447 221.79 ug/L Kr 83 2241.632 3.370 -263.071 ug/L Ag 107 130.669 3.093 -0.000 -0.01377 2.02 ug/L In 115 1628980.270 0.260 1628980.270 ug/L Sb 121 549.689 5.095 0.000 0.05154 5.67 ug/L Sb 123 423.070 5.650 0.000 0.05139 6.15 ug/L Ba 135 57398.233 1.603 0.021 16.68536 1.00 ug/L Ba 137 100473.640 1.933 0.038 16.60617 0.64 ug/L > Tb 159 2672326.647 1.297 2672326.647 ug/L Hg 201 45.667 23.001 -0.000 -0.00027 2248.27 ug/L Hg 202 96.668 14.967 0.000 0.00032 1178.42 ug/L TI 205 900.054 4.523 -0.000 -0.00129 57.14 ug/L Pb 208 11414.916 0.585 0.003 0.17038 1.73 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 79.676 Cr 52 Cr 53 Mn 55

Sample ID: AE09970 Report Date/Time: Tuesday, May 14, 2002 11:35:00 Page 1

NYC-WTC_000053462

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