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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09153 Sample Date/Time: Wednesday, May 08, 2002 11:46:21 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE091 53.790 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 9.333 32.733 -0.000' -0.00401 200.99 ug/L Se-1 45 475254.302 1.207 475254.302 ug/L Cr 52 8505.396 1.215 0.002 0.08990 19.29 ug/L Cr 53 1243.431 2.817 0.001 0.35981 6.73 ug/L Mn 55 268635.188 2.989 0.552 15.02310 3.57 ug/L Ni 60 1133.415 2.831 0.002 0.37300 3.40 ug/L Cu 63 45817.318 1.895 0.096 7.30148 2.72 ug/L Cu 65 22441.238 2.932 0.047 7.26684 3.98 ug/L Zn 66 3976.577 4.895 0.026 1.56715 4.69 ug/L Zn 67 782.708 3.157 0.005 1.64664 0.17 ug/L Zn 68 3576.740 3.016 0.024 1.88329 0.65 ug/L Ge 72 124584.029 3.288 124584.029 ug/L As 75 12547.942 1.593 0.011 0.52428 15.97 ug/L Se 77 1563.393 0.609 0.001 0.35772 71.53 ug/L Se 82 42.295 311.975 0.001 0.36042 130.82 ug/L Kr 83 4302.061 2.270 -159.411 ug/L Ag 107 204.004 4.188 -0.000 -0.01328 5.33 ug/L in 115 1857269.795 1.978 1857269.795 ug/L Sb 121 642.362 1.258 0.000 0.04099 3.53 ug/L Sb 123 539.495 3.502 0.000 0.04486 6.71 ug/L Ba 135 60066.075 1.427 0.022 15.25445 0.87 ug/L Ba 137 104558.567 0.545 0.039 15.16455 0.69 ug/L > Tb 159 2681437.249 1.057 2681437.249 ug/L Hg 201 145.669 5.716 0,000 0.01154 46.04 ug/L Hg 202 290.674 5.400 0.000 0.00585 72.37 ug/L TI 205 1157.085 3.226 -0.000 -0.01159 5.56 ug/L Pb 208 20100.207 1.628 0.006 0.31466 1.18 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery , Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 92.939 Cr 52 Cr 53 Mn 55

Sample ID: AE09153 Report Date/Time: Wednesday, May 08, 2002 11:48:01 Page 1

NYC-WTC_000053123

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