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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09653 Sample Date/Time: Tuesday, May 14, 2002 10:18:40 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09653.020 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 11.667 40.507 0.000' 0.00649 156.12 ug/L Se-1 45 585643.845 2.225 585643.845 ug/L Cr 52 10280.246 1.397 0.002 0.11678 13.04 ug/L Cr 53 2332.656 0.398 0.003 1.00100 2.83 ug/L Mn 55 382685.219 2.242 0.652 18.15270 0.91 ug/L Ni 60 1050.405 1.243 0.002 0.32673 1.39 ug/L Cu 63 6843.644 2.291 0.011 0.98528 0.72 ug/L Cu 65 3264.286 3.095 0.005 0.97944 3.16 ug/L Zn 66 2834.137 2.030 0.014 0.83311 2.29 ug/L Zn 67 745.705 3.501 0.004 1.44520 3.70 ug/L Zn 68 2823.134 3.995 0.016 1.25746 3.94 ug/L Ge 72 128481.927 1.322 128481.927 ug/L As 75 6868.357 2.576 0.009 0.43234 7.68 ug/L Se 77 960.453 2.970 0.001 0.49081 13.21 ug/L Se 82 -20.572 564.392 -0.000 -0.02470 1613.13 ug/L Kr 83 2327.321 3.348 -177.382 ug/L Ag 107 157.670 2.563 -0.000 -0.01231 3.12 ug/L In 115 1699199.598 1.254 1699199.598 ug/L Sb 121 564.023 3.638 0.000 0.05063 2.94 ug/L Sb 123 421.536 3.574 0.000 0.04892 4.40 ug/L Ba 135 56585.169 2.020 0.021 16.21310 1.84 ug/L Ba 137 98617.705 1.111 0.036 16.06676 0.98 ug/L Tb 159 2711077.302 0.428 2711077.302 ug/L Hg 201 54.334 14.990 0.000 0.00449 104.63 ug/L Hg 202 116.002 4.800 0.000 0.00498 31.17 ug/L Tl 205 1025.735 4.130 0.000 0.00147 67.64 ug/L Pb 208 4720.194 2.969 0.001 0.03473 6.86 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff Be 9 > Sc-1 45 83.105 Cr 52 Cr 53 Mn 55

Sample ID: AE09653 Report Date/Time: Tuesday, May 14, 2002 10:20:21 Page 1

NYC-WTC_000053428

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