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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09333 Sample Date/Time: Wednesday, May 08, 2002 12:52:17 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09333.801 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 18.667 34.022 0.000' 0.02216 78.06 ug/L Se-1 45 461462.122 1.698 461462.122 ug/L Cr 52 8595.481 1.449 0.003 0.12322 14.94 ug/L Cr 53 1572.152 3.245 0.002 0.66077 9.68 ug/L Mn 55 520656.351 0.929 1.115 30.35792 0.85 ug/L Ni 60 2585.393 1.146 0.005 0.92156 1.46 ug/L Cu 63 83751.183 0.122 0.181 13.77967 1.65 ug/L Cu 65 40896.537 1.454 0.088 13.68460 1.10 ug/L Zn 66 8411.975 1.489 0.064 3.84876 2.73 ug/L Zn 67 1532.811 0.685 0.011 3.79250 1.10 ug/L Zn 68 6876.669 1.284 0.052 4.13104 1.02 ug/L > Ge 72 120551.971 1.147 120551.971 ug/L As 75 11701.904 2.783 0.007 0.34680 42.83 ug/L Se 77 1468.403 2.903 0.000 0.15713 139.84 ug/L Se 82 -67.784 125.234 -0.000 -0.03068 1018.44 ug/L Kr 83 4113.305 0.352 -348.168 ug/L Ag 107 615.360 7.648 0.000 0.01429 19.50 ug/L > In 115 1782402.469 0.923 1782402.469 ug/L Sb 121 1119.414 10.671 0.001 0.08217 10.91 ug/L Sb 123 814.598 4.438 0.000 0.07665 4.42 ug/L Ba 135 68496.779 0.947 0.026 17.69427 1.11 ug/L Ba 137 118927.439 1.205 0.045 17.54324 0.96 ug/L > Tb 159 2636917.679 2.058 2636917.679 ug/L Hg 201 235.339 6.909 0.000 0.06273 17.59 ug/L Hg 202 527.021 10.447 0.000 0.06500 18.74 ug/L TI 205 1171.087 8.222 -0.000 -0.01078 18.92 ug/L Pb 208 56652.138 0.893 0.020 1.00260 2.04 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Sc-1 45 90.242 Cr 52 Cr 53 Mn 55

Sample ID: AE09333 Report Date/Time: Wednesday, May 08, 2002 12:53:59 Page 1

NYC-WTC_000053145

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