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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09576 Sample Date/Time: Wednesday, May 08, 2002 15:17:38 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09576.831 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 9.667 5.973 -0.000- -0.00141 170.99 ug/L Sc-1 45 446345.036 3.033 446345.036 ug/L Cr 52 11327.834 1.474 0.009 0.43148 7.19 ug/L Cr 53 2285.644 1.269 0.003 1.31257 6.22 ug/L Mn 55 288621.463 1.418 0.633 17.25109 4.08 ug/L Ni 60 898.053 4.635 0.002 0.30930 1.81 ug/L Cu 63 62529.603 0.414 0.140 10.63273 3.26 ug/L Cu 65 30894.717 0.431 0.069 10.68177 3.14 ug/L Zn 66 7506.507 2.382 0.059 3.57732 2.41 ug/L Zn 67 1381.452 3.729 0.011 3.55902 4.44 ug/L Zn 68 6040.400 1.228 0.048 3.77342 1.44 ug/L > Ge 72 114976.318 0.214 114976.318 ug/L As 75 10640.772 1.312 0.003 0.12797 51.61 ug/L Se 77 1376.521 2.176 0,000 0.04544 322.71 ug/L Se 82 22.673 143.180 0.001 0.30585 40.92 ug/L Kr 83 3643.433 0.848 -818.039 ug/L Ag 107 167.003 4.521 -0.000 -0.01438 3.86 ug/L > in 115 1660573.983 0.711 1660573.983 ug/L Sb 121 600.026 4.770 0.000 0.04323 5.64 ug/L Sb 123 470.697 2.644 0.000 0.04348 3.97 ug/L Ba 135 53359.684 1.038 0.021 14.02558 1.30 ug/L Ba 137 92636.516 0.335 0.036 13.90541 1.24 ug/L > Tb 159 2590776.557 1.363 2590776.557 ug/L Hg 201 73.334 15.805 -0.000 -0.02650 26.75 ug/L Hg 202 166.670 3.995 -0.000 -0.02273 4.81 ug/L n 205 681.032 5.163 -0.000 -0.02260 2.90 ug/L Pb 208 36632.901 1.210 0.013 0.64129 0.37 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 87.286 Cr 52 Cr 53 Mn 55

Sample ID: AE09576 Report Date/Time: Wednesday, May 08, 2002 15:19:19 Page 1

NYC-WTC_000053203

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