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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09764 Sample Date/Time: Tuesday, May 14, 2002 10:21:41 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09764.021 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 10.667 14.321 0.000 - 0.00488 72.23 ug/L Se-1 45 572027.875 1.480 572027.875 ug/L Cr 52 9720.960 1.876 0.002 0.09039 5.45 ug/L Cr 53 2297.647 0.979 0.003 1.01392 1.16 ug/L Mn 55 396750.976 0.204 0.692 19.27332 1.35 ug/L Ni 60 1079.742 1.748 0.002 0.34445 1.94 ug/L Cu 63 7818.773 1.152 0.013 1.16095 2.45 ug/L Cu 65 3719.131 2.110 0.006 1.15101 2.89 ug/L Zn 66 1804.531 2.290 0.006 0.38000 2.53 ug/L Zn 67 515.020 1.359 0.003 0.87429 3.98 ug/L Zn 68 2038.916 1.913 0.010 0.80494 4.90 ug/L Ge 72 125564.871 1.182 125564.871 ug/L As 75 6773.382 2.431 0.009 0.45683 18.82 ug/L Se 77 939.310 3.800 0.001 0.49537 37.58 ug/L Se 82 10.558 808.986 0.000 0.08803 342.92 ug/L Kr 83 2274.974 2.903 -229.730 ug/L Ag 107 149.003 8.776 -0.000 -0.01263 7.97 ug/L In 115 1655578.986 1.915 1655578.986 ug/L Sb 121 550.022 1.012 0.000 0.05070 2.48 ug/L Sb 123 424.833 3.118 0.000 0.05076 5.13 ug/L Ba 135 56490.200 0.315 0.021 16.63355 0.57 ug/L Ba 137 98710.017 0.888 0.037 16.52638 1.00 ug/L > Tb 159 2638250.274 0.258 2638250.274 ug/L Hg 201 56.667 18.536 0.000 0.00681 93.31 ug/L Hg 202 117.002 7.451 0.000 0.00607 37.09 ug/L TI 205 1042.737 2.930 0.000 0.00260 32.23 ug/L Pb 208 4840.886 1.625 0.001 0.03976 4.63 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 81.173 Cr 52 Cr 53 Mn 55

Sample ID: AE09764 Report Date/Time: Tuesday, May 14, 2002 10:23:22 Page 1

NYC-WTC_000053430

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