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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09579 Sample Date/Time: Tuesday, May 14, 2002 10:03:31 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd 1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09579.015 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 10.000 36.056 0.000' 0.00384 210.59 ug/L > Se-1 45 563235.857 1.609 563235.857 ug/L Cr 52 10321.293 0.810 0.003 0.15283 9.95 ug/L Cr 53 2368.666 3.117 0.003 1.08880 6.40 ug/L Mn 55 729311.468 1.821 1.293 36.02618 1.59 ug/L Ni 60 1430.460 0.718 0.002 0.46763 2.35 ug/L Cu 63 57128.900 2.161 0.101 8.92600 2.48 ug/L Cu 65 27318.606 2.345 0.048 8.91737 3.65 ug/L Zn 66 10552.227 1.402 0.077 4.51802 2.18 ug/L Zn 67 1863.210 1.399 0.013 4.51024 2.31 ug/L Zn 68 8399.296 0.162 0.061 4.84137 0.77 ug/L Ge 72 124764.586 0.849 124764.586 ug/L As 75 6883.638 1.799 0.011 0.51619 6.68 ug/L Se 77 943.338 2.162 0.001 0.53699 22.05 ug/L Se 82 -26.828 153.772 -0.000 -0.04641 314.98 ug/L Kr 83 2318.319 0.840 -186.385 ug/L Ag 107 565.690 1.203 0.000 0.01672 3.26 ug/L In 115 1653393.612 1.722 1653393.612 ug/L Sb 121 760.373 4.291 0.000 0.07132 2.81 ug/L Sb 123 604.542 4.684 0.000 0.07390 3.11 ug/L Ba 135 54499.757 0.787 0.021 16.09113 0.23 ug/L Ba 137 95358.828 0.843 0.036 16.00875 0.25 ug/L Tb 159 2630985.589 0.793 2630985.589 ug/L Hg 201 88.001 9.709 0.000 0.02603 19.03 ug/L Hg 202 180.004 13.135 0.000 0.02298 26.27 ug/L TI 205 1156.085 4.501 0.000 0.00554 26.51 ug/L Pb 208 25555.322 1.383 0.009 0.46203 1.43 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 79.925 Cr 52 Cr 53 Mn 55

Sample ID: AE09579 Report Date/Time: Tuesday, May 14, 2002 10:05:12 Page 1

NYC-WTC_000053418

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