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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09329 Sample Date/Time: Wednesday, May 08, 2002 11:59:04 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09329.794 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 11.667 38.651 0.000 0.00227 507.87 ug/L > Se-1 45 471764.629 1.894 471764.629 ug/L Cr 52 8508.732 0.495 0.002 0.09630 14.34 ug/L Cr 53 1398.788 1.466 0.001 0.49270 7.51 ug/L Mn 55 317375.795 1.042 0.659 17.95431 2.71 ug/L Ni 60 1089.410 7.875 0.002 0.35984 7.04 ug/L Cu 63 7406.424 1.656 0.015 1.15667 0.67 ug/L Cu 65 3645.434 1.386 0.007 1.14245 1.73 ug/L Zn 66 1828.536 3.330 0.009 0.54678 8.00 ug/L Zn 67 525.020 3.182 0.003 0.98588 6.44 ug/L Zn 68 1831.870 1.015 0.010 0.79600 2.39 ug/L > Ge 72 122090.365 1.502 122090.365 ug/L As 75 11719.094 1.291 0.006 0.29433 20.18 ug/L Se 77 1460.072 1.523 0.000 0.03836 130.90 ug/L Se 82 -101.243 50.602 -0.000 -0.14836 123.28 ug/L Kr 83 4164.329 0.675 -297.144 ug/L Ag 107 88.001 13.398 -0.000 -0.02037 3.53 ug/L > In 115 1778166.645 1.062 1778166.645 ug/L Sb 121 587.358 6.845 0.000 0.03872 9.13 ug/L Sb 123 476.946 5.530 0.000 0.04058 7.96 ug/L Ba 135 57269.743 1.135 0.022 14.78416 1.87 ug/L Ba 137 99152.139 1.053 0.038 14.61615 1.38 ug/L > Tb 159 2638141.491 0.969 2638141.491 ug/L Hg 201 72.001 25.345 -0.000 -0.02800 37.20 ug/L Hg 202 127.336 8.324 -0.000 -0.03313 7.32 ug/L TI 205 996.398 8.061 -0.000 -0.01509 14.09 ug/L Pb 208 5787.786 1.375 0.001 0.05401 3.26 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Sc-1 45 92.257 Cr 52 Cr 53 Mn 55

Sample ID: AE09329 Report Date/Time: Wednesday, May 08, 2002 12:00:44 Page 1

NYC-WTC_000053131

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