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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09768 Sample Date/Time: Tuesday, May 14, 2002 11:15:09 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd 1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\AE09768.031 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 11.667 19.795 0.000 ' 0.00731 70.47 ug/L Sc-1 45 565131.528 0.799 565131.528 ug/L Cr 52 10595.946 2.334 0.004 0.17263 14.28 ug/L Cr 53 3008.195 3.390 0.004 1.52903 5.51 ug/L Mn 55 576635.120 0.992 1.018 28.37816 1.78 ug/L Ni 60 1564.150 0.966 0.003 0.51059 1.44 ug/L Cu 63 68367.467 0.610 0.120 10.65481 1.38 ug/L Cu 65 32926.188 1.301 0.058 10.71888 1.58 ug/L Zn 66 3967.572 1.508 0.025 1.44703 3.34 ug/L Zn 67 902.721 0.448 0.006 1.97718 1.64 ug/L Zn 68 3670.778 0.526 0.024 1.89548 1.23 ug/L > Ge 72 122191.648 1.021 122191.648 ug/L As 75 6805.152 3.674 0.011 0.54222 21.89 ug/L Se 77 961.789 5.736 0.001 0.69994 35.56 ug/L Se 82 43.819 123.783 0.000 0.20841 94.22 ug/L Kr 83 2207.623 1.119 -297.080 ug/L Ag 107 332.343 6.890 0.000 0.00079 241.39 ug/L > In 115 1619325.222 1.215 1619325.222 ug/L Sb 121 703.368 7.041 0.000 0.06718 6.13 ug/L Sb 123 547.793 8.687 0.000 0.06807 7.89 ug/L Ba 135 64439.918 1.374 0.024 18.70101 0.96 ug/L Ba 137 112035.316 1.290 0.042 18.48706 0.84 ug/L > Tb 159 2677000.930 0.487 2677000.930 ug/L Hg 201 79.334 14.932 0.000 0.01992 35.96 ug/L Hg 202 187.670 1.231 0.000 0.02419 2.53 ug/L TI 205 932.724 2.671 -0.000 -0.00052 103.11 ug/L Pb 208 14666.459 0.080 0.004 0.23507 0.65 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 80.194 Cr 52 Cr 53 Mn 55

Sample ID: AE09768 Report Date/Time: Tuesday, May 14, 2002 11:16:50 Page 1

NYC-WTC_000053450

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