GCMS analysis results for sample AE01333, Feb 2002

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Data File : C:\HPCHEM\l\DATA\FEB1902\1333.D Vial: 7 Acq On : 19 Feb 2002 4:15 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.37 ug/1 24920 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl formamide 73 C3H7NO 000627-45-2 5 2 1,3 -Dioxolane 74 C3H602 000646-06-0 4 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 4 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-2 4 Abundance / Scan 344 (8.204 min): 1333.D (-) ...m/z73.00 100.00%’ 73

5000 43 40 7.80 8.00 8.20 8.40 8.60 86 55 .. 7. 69 TTTTT 43.05 31.51%

A 3‘‘7111 ............................................ p-n-TT 1 T 11 ■ •" i ■ ।" i11" । ” । ■ p' m/ z 1Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 j Abundance #292: N-Ethylformamide 30 73

5000 53 7.80 8.00 8.20 8.40 8.60 | 44 27 m/z— 39,95—w—.13-396 15

m/z-> h''' np 5 — yMirjkin T’’" n —41++ i1 ■" i11" P''11 i- ‘ ■ i 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 j Abundance 73 29 44 7.80 8.00 8.20 8.40 8.60 5000 m/ z 45.05 11.55% 15 19 26 i1'1' I'1'11 ■1'11" 11111111" " i" " r'1' r "1111'11' ‘1111''' I •11 ■ I ■1 ■' i1"11' " ■ I'1'11111111 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #763: 1-Butanamine, 3-methyl- 3k) 7J0_8.00__ 8.20 8.40 8.60 m/z 41.05 10.94% 5000

15 27 ,4144 55 58 70 87 TMmmPTTTTTTT T1g—3mnpT TTTTT i1'111 TTTTT ‘T m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1333.D GCMS0208.M Thu Feb 21 15:26:39 2002 Page 1

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