GCMS blank analysis results for sample AE01330, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1902\LB.D Vial: 3 Acq On : 19 Feb 2002 11:13 am Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) * Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.37 ug/1 26543 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-Ethylformamide 73 C3H7NO 000627-45-2 5 2 1-Hexanol, 6-amino- 117 C6H15NO 004048-33-3 4 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC1302 000000-00-0 4 4 1-Octanamine 129 C8H19N 000111-86-4 4 Abundance ■ Scan 345 (8.207 min): LB.D (-) m/z 73.00 100. 00% 7b

5000 43 55 86 7.80 8.00 8.208.40__8.60 1 1 1 l'1 11 ' I 1 ' ' 1 1' l ■ ■ । ■ I' ■ i ■ > • ■ i ■ ■ ■ ■ t > ■ ■ ■ i > m/z 43.05 2 7/88% m/z—2 10 20 30 40 50 60 70 80 90 100 110 120 Ssi - ' L #292: N-Ethylformamide 30 73

5000 44 58 7.80 8.00 8.20 8.40 8.60 m/z 45.05 10.17%

1 1 TTTi |_r ■ 1 11 1 ■ ■ i 1 41—— m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abunerco 30

7.80 8.00 I 8.20 A8.40 8.60 5000 m/z 41.05 9.77%

45 66 72 81 87 100 IIBn—pnmmkm——nmm//u/d m/z- 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet ' I ■ ■ ■ 1 i ' 1 ' ' i ■ ■ ■ ' i • ' 733 7.80 8.00__ 8.20 8.40 8.60 m/z 71.00 7.00% 5000

45 36 I | 1 ' i ' 1 ' ' I ' ■ ■ ■ i ■ ' 1 1 55 67 ,109,15, 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40 8.60

LB.D GCMS0208.M Thu Feb 21 15:31:17 2002 Page 1

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