NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\l\DATA\FEB1902\1404.D Vial: 13
Acq On : 19 Feb 2002 10:03 pm Operator: 209 GALOS
Sample : gc/ms scan 1/18 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 N-Ethylformamide Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.21 0.30 ug/1 25097 1,4-Dichlorobenzene-d4 12.33
Hit# of 5 / Tentative ID MW MolForm CAS# Qual
1 N-Ethyl fprmamide 73 C3H7NO 000627-45-2 5
2 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 5
3 1,3 -Dioxolane 74 C3H602 000646-06-0 5
4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4
Abuss nee Scan 345(8.209 min): 1404.D (-) ' m/z 73.00 100.00 %
78
5000
43
55 87 103 7.80 8.00 8.20 8.40 8.60
■ ' i ' ' ' ' I 1 1 ' ■ i ' ' in LL
dr 10011*— ■ 1 ( r- m/z 43 .05 29.73%
m/z-> 10 20 30 40 50 60 70 80 90 100 110
Abu d nice #292: N-Ethylformamide
30
73
5000
A
I ' ' 1 ’ 1 • '
58 7.80 8.00 8.20 8.40 _8.60
44
m/ z 40.95 11.39%
miz->
1 ' i
10 20
130 ' i'ii .
40
। .
50
.
60 70 80 90 100 110
Abundance
30
7.80 8.00 8.20 8.40 8.60
5000 m/ z 45.05 11.16%
44
15 56 87
■ ■ l ■ • ■ ■ l ryn-n-r-r-y-r-r-r-1 —p > • i • • • • i ■ ■
Abim, nr.)
10 20 30 40 50 60 70
#62555: 1,3-bioxolane
73
80 90 100 110
....... It
7.80 8.00 8.20 8.40 8.60
m/z 71.00 7.62%
5000 44
29
- 57 68
1 1 1 1 ' 1 1 1 1 1 1 1 1 1
m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60
1404.D GCMS0208.M Thu Feb 21 15:30:13 2002 Page 1
NYC-WTC_000052960
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