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GCMS analysis results for sample AE01404, Feb 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01404 conducted on February 27, 2002.

NYC-WTC_000052953–000052961

Folder label: “GCMS X 1/10/02 A 2/19/02

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Scanned page image, NYC-WTC_000052960
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1902\1404.D Vial: 13 Acq On : 19 Feb 2002 10:03 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.30 ug/1 25097 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 N-Ethyl fprmamide 73 C3H7NO 000627-45-2 5 2 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 5 3 1,3 -Dioxolane 74 C3H602 000646-06-0 5 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 Abuss nee Scan 345(8.209 min): 1404.D (-) ' m/z 73.00 100.00 % 78

5000 43

55 87 103 7.80 8.00 8.20 8.40 8.60 ■ ' i ' ' ' ' I 1 1 ' ■ i ' ' in LL dr 10011*— ■ 1 ( r- m/z 43 .05 29.73% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abu d nice #292: N-Ethylformamide 30 73

5000 A I ' ' 1 ’ 1 • '

58 7.80 8.00 8.20 8.40 _8.60 44 m/ z 40.95 11.39%

miz-> 1 ' i 10 20 130 ' i'ii . 40 । . 50 . 60 70 80 90 100 110 Abundance 30

7.80 8.00 8.20 8.40 8.60 5000 m/ z 45.05 11.16% 44 15 56 87 ■ ■ l ■ • ■ ■ l ryn-n-r-r-y-r-r-r-1 —p > • i • • • • i ■ ■

Abim, nr.) 10 20 30 40 50 60 70 #62555: 1,3-bioxolane 73 80 90 100 110 ....... It 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.62% 5000 44

29 - 57 68 1 1 1 1 ' 1 1 1 1 1 1 1 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1404.D GCMS0208.M Thu Feb 21 15:30:13 2002 Page 1

NYC-WTC_000052960

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NYC-WTC_000052960Source: NYC Law Department, mirrored locally

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