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GCMS comments for sample AD29789 showing no unusual compounds, Jan

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Laboratory commentary noting a GCMS scan of sample AD29789 revealed no unusual compounds on January 9, 2002.

NYC-WTC_000037135–000037145

Folder label: “GCMS X 12/10/01 A 12/15/01

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Scanned page image, NYC-WTC_000037142
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NYC 9/11 Public Portal Document

• Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29789.D Vial: 21 Acq On : 15.Dec 2001 10:02 pm Operator: 209 GALOS Sample : gcms scan 12/10 a Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********************************************************************

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 7.59 4.00 ug/1 1094710 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual ---------------- ---------------------------------------------------- 1 N-Ethylfor mide 73 C3H7NO 000627-45-2 9 2 1,3-Diox ane, 2-(3-bromo-5,5,5-tri 352 C10H16BrCl3O2 000000-00-0 9. 3 Butane 2-methoxy-2-methyl- 102.C6H14O 000994-05-8 9 4 Silari , tetramethyl- 88 C4H12Si 000075-76-3 5 Abundance Scan 278 (7.594 min): 29789.D (-) m/z 73. O0 100.00

5000

87 7.20 7.40 7.60 7.80 8.00 3 55 0 67 103 m/z 43.00 27.68, 10 20 30 40 50 60 70 80 90 100 110 120 dance #292: N-Ethylformamide

73

5000 7.20 7.40 7.60 7.80 8.00 44 58 m/z 41.00 10.42 15 ,

> 10 20 30 40 50 60 70 80 90 100 110 120 dance #49423: 1,3-Dioxolane, 2-(3-brorno-5.5,5-trichloro-2,2-dimes 73

7.20 7.40 7.60 7.80 8.00 5000 m/z 44.90 10.041 45 36 55 67 109 115 > 10 20 30 40 50 60 70 80 90 100. 110 120 dance #1761: Butane, 2-methoxy-2-methyl- 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.471 5000 55 87 27 33 45

} 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29789.D GCMS1126.M Fri Dec 28 13:24:49 2001 Page 1

NYC-WTC 000037142

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NYC-WTC_000037142Source: NYC Law Department, mirrored locally

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