Technical document listing calibration standards and response factors for gas chromatography-mass spectrometry analysis of TCLP samples in February 2002.
NYC-WTC_000052884–000052891Folder label: “GCMS X 1/10/02 A 2/19/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\1\DATA\FEB1902\1231.D Vial: 6 Acq On : 19 Feb 2002 3:17 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.22 0.39 ug/1 28021 1,4-Dichlorobenzene-d4 12.34
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-Ethylformaraide 73 C3H7NO 000627-45-2 9 2 Butane, 2-methoxy-2-methyl - 102 C6H140 000994-05-8 9 3 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 4 1-Butanamine, 3-methyl- 87 C5H13N 100.00% 7 000107-85-7 Abundance................ ’............... Scan 346 (8.217 min): 1231.D(-) m/ z 73.00 73
5000 43 7.80 8.00 8.20 8.40 8.60 - 571 87 W3 m/ z 26.48% m.z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #292: N-Ethylformamide 300 73
5000 7.80 A 8.00 8.20 AA— 8.40__ 8.60 14 58 m/ z 41.05 11.33% .......... . ... ...... ... ..... ... .......... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance , 73
7.80 8.00 8.20 8.40 8.60 5000- m/ z 71.00 8.48% 55 87
m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191:1,3-Dioxolane. 2-pentadecyl 43 7.80 8.00 8.20 8.40 8.60 m/z 45.05 8.15% 5000
m/z—> .... 43 57 . ' I ' ' • ' I ‘ TdT 20 40 60 86 99 256 283 80 100 120 140 160 180 200 220 240 260 280 .. ..... 11 1 7.80 8.00 8.20 8.40 8.60
1231.D GCMS0208.M Thu Feb 21 15:24:40 2002 Page 1
NYC-WTC_000052889
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NYC-WTC_000052707
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052644
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052600
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052630
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052586
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052714
Calibration table and instrument data for GC/MS analysis generated on February 12 and 19, 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052614
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052701
Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052726
GC/MS analysis report for sample AE01036 showing surrogate recovery data generated on February 26, 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052815
GC/MS analysis report for sample AE01225 showing surrogate recovery data generated on February 25, 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052805
GC/MS analysis report for sample AE01226 showing surrogate recovery data generated on February 25, 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006371
Initial GCMS analysis report for sample AE01940 conducted by analyst DLV on March 13, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000052848
Fragmented page from a Department of Environmental Protection laboratory record dated February 2002.
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NYC-WTC_000052849
Technical document containing metadata and header information for a gas chromatography-mass spectrometry analysis from February 2002.
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NYC-WTC_000052852
Laboratory report showing calibration data for multiple organic compounds analyzed in sample AE01330 on February 19, 2002.
Filed in the same folder
NYC-WTC_000052855
Laboratory report documenting reference standard analysis for organic compounds in sample AE01330 conducted on February 19, 2002.
Filed in the same folder
NYC-WTC_000052860
Laboratory report documenting blank analysis for organic compounds in sample AE01330 to verify analytical system cleanliness on February 21, 2002.
Filed in the same folder