GCMS analysis results for sample AE01402, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1902\1402.D Vial: 11 Acq On : 19 Feb 2002 8:07 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.33 ug/1 27043 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Butane, /2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 4 Octanal, 7-methoxy-3,7-dimethyl- 186 C11H2202 003613-30-7 4 Ab u dance / Scan 345(8.211 min): 1402.D(-) : m/z 73.00100.00% 73

5000 43 7.80 8.00 8.20 8.40 8.60 i ' ' ' ' i 4414,57. । । nr | 37 103 m/z 43.05 28.48% m/- 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

/ YA A 5000 58 7.80 8.00 8.20 8.40 8.60 44 m/ z 41.05 12.18% ■ ■ I » ■ i > • ■ > । . . . > । i .') . । . m/z- 10 20 30 40 50 60 70 80 90 100 110 Abundance 73 ..... 1}........ 7.80 8.00 8.20 8.40 8.60 5000- 55 m/ z 45.05 9.45% 87 27 45 ........... 33 ■ i ■ ■ ■ • i ■ • ■ ■ i ■ ■ ■ ■ i ■ • ■ . । ■ i ■ ■ ■ ■ i ■ ■ ■ i I 1 m/z- 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30 7.80 8.00 _ 8.20 8.40 8.60 m/z 71.00 7.49% 5000

15 41 , 55 70 87 —.............................................. ’ 1 1 1 ’1' 1 1 ' ' ■ ■ ■ । i 1 -i—> ■ r • ■ • > > । » 1 1 > । 1 ■ । 1 । । m/z- 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1402.D GCMS0208.M Thu Feb 21 15:28:58 2002 Page 1

NYC-WTC_000052925