GCMS calibration table for TCLP analysis, Feb 2002

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Technical document listing calibration standards and response factors for gas chromatography-mass spectrometry analysis of TCLP samples in February 2002.

NYC-WTC_000052884–000052891

Folder label: “GCMS X 1/10/02 A 2/19/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1902\1231.D Vial: 6 Acq On : 19 Feb 2002 3:17 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP.calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Benzoic acid, 2-[(trimethylsil Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.93 0.22 ug/1 21461 Naphthalene-d8 15.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 33 2 Cyclopentsiloxane, 000541-02-6 33 decamethyl- 370 C10H3005Si5 3 Phenethyl amine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 23 4 Benzeneethanamine , N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 23 Abur: ro / Scan 1077 (14.928 min): 1231.D(-) m/z 73.00 100.00% 3

5000 207 355 45 ■193 14.60 14.80 15.00 15.20 |, m/z-> 'i ■‘ ' 'r TT T 1WTTTPPWTIIWTIPTTTITTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ‘‘ ‘I 1 11'' I m/z 266.90 38.71% Abundance #72300: Benzoic acid. 2-[(trimethylsilyijoxy]-. trimethylsi 3

267 5000- 14.60 14.80 15.00 15.20 45 T 0 .■ 28.51% 92 135151 175 193 209 233 249 i * ■' • i i ■ ■ ■ ■ i '' ■ ■ i '' ' ■ i •'' ■ i ■'' ■ i ’ ■ ' ' i' ■ ' • i i11 ■ ■ i' ■ ■ ■ i ■ ■ • ■ i T" m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 33

14.60 14.80 15.00 15.20 267 5000 m/z 73.90 10.15%

191 207 251 323 339 I ' ’ ’' I I'''' I''' TT7T i ■' ■11 Ti11'■n’ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-niethyl-.beta.,3,4-tris(trimethyls 14.60 14.80 15.00 15.20 m/z 356.05 10.15% 5000 355 44 |, 88 130 147 193 267 294 TT TTT i1 ■ ■-1 ■11 ' ■' I TTTT .............. TH m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

1231.D GCMS0208.M Thu Feb 21 15:24:45 2002 Page 2

NYC-WTC_000052890

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