GCMS analysis results for sample AE01047, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\022802\01047FB.D Vial: 16 Acq On : 28 Feb 2002 11:15 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst Instrumen • Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 4(1H)-Pteridinone, 6-acetyl... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

37.54 0.44 ug/L 106344 Perylene-d12 34.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4(1H)-Pteridinone, 6-acetyl-2-am... 207 C8H9N5O2 042310-08-7 38 2 2-Imino-3-phenyl-4-thiazolidinone 192 C9H8N20S 000000-00-0 32 3 3,7-Dimethyl-lH-pyrimido[l,2-a)p... 191 C9H9N3O2 000000-00-0 25 4 .beta. N METHYL IONONE 206 C14H22O 000127-43-5 16 Abundance Scan 3800 (37.543 min): 01047FB.D (-) m/z 191.15 100.00% 191

95 A

55 5000 68 119 135 151 177 was MA 81 163 105 37.20 37.40 37.60 37.80

m/z-> 0 r 1 1 ' 60 LL— 80 100 120 140 160 180 200 LX 205 m/z 95.10 73.79%

Abundance #125157: 4(1H)-Pteridinone, 6-acetyl-2-amino-7.8-dihydro-... 191 Aw Www 5000 205 37.20 37.40 37.60 37.80 177 136 162 m/z 55.10 53.84%

m/z-> Abundance 0 60 80 100 106 120 LL 4-l149—44l| 120 140 160 180 #102230: 2-l mino-3-phenyl-4-thiazolidinone TT

191 200 Pr Vwws 37.20 37.40 37.60 37.80 118 m/z 135.10 37.89% 5000

W 135 164 V 0- Trk pi l ' r m/z—> 60 80 100 120 140 160 180 200 Abundance #101303: 3,7-Dimethyl-1 H-pyrimido[1,2-a]pyrimidine-2,8-dione 191 TT 37.20 37.40 37.60 37.80 m/z 151.20 36.48%

5000 151 69 122 163 54 82 95 134 0 Ttdir ,........ I, , I, , , ' ■ i 1 ' ■ ' i ‘ ■ — m/z-> 60 80 100 120 140 160 180 200 37.20 37.40 37.60 37.80

01047FB.D 5080202.M Wed Mar 13 11:03:38 2002 Page 7

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