GCMS analysis results for sample AE00472, Feb 26 2002

NYC 9/11 Public Portal Document Library searci LompU

.Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Penten-2-ol $$ .alpha.,.g... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.71 0.14 ug/L 63749 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol $$ .alpha.,.gamma.... 86 C5H10O 001569-50-2 64 2 3-Penten-2-ol 86 C5H10O 001569-50-2 50 3 3-PENTEN-2-OL, (Z)- 86 C5H10O 024652-50-4 50 4 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 40 Abundance Scan 205 (5.714 min): 00472A.D (-) m/2 41.10 100.00% 41 71

5000 45 84 A............ 3& 58 5.40 5.60 5.80 6.00 — - m/z 43.10 92.31% 0 11 ■ ‘1' ।1 1′0010101 rn/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4047:3-Penten-2-ol $$ .alpha.,.gamma.-Dimethylallyl alco... 43 71

5000 39 TT 4,T 27 53 5.40 5.60 5.80 6.00 67 m/z71.10 81.94% 58 86 - 49 - 1111'11''1 ■ i ■ ■ ’ ■ i 01 ■n-f-r-m-j-r ■11'' TTT । 11 I r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4046: 3-Penten-2-ol 7h 43 T 5.40 5.60 5.80 6.00 5000 39 m/Z 69.10 50.76% 53 67 27 58 86 0 ■ ■ i'''' i' 1 Muni rl ITTT H m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4208:3-PENTEN-2-OL, (Z)- ■ ■ i ■ ' ■ ■ I 7h 5.40 5.60 5.80 6.00 43 m/ Z 39.10 43.95%

5000 39 53 67 27

n/z-> 0 ■ ■ 11‘ l ■ 20 25 • < I'' ‘111'1 30 35 + 40 45 11111 50 • i ■ ’1 ■ i ■ •" i ■

55 58

60 65 70 —- 75 80 86

85 90 95 5.40 ....... ................. ......... 5.60 5.80 6.00

00472A.D HP020702.M Thu Feb 21 09:57:54 2002 Page 7

NYC-WTC_000052281