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GCMS analysis results for sample AE00472, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00472, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052271–000052290

Folder label: “GCMS X 1/11/02 A 2/7/02

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NYC 9/11 Public Portal D ocument Library Searcn Compo uiu

Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 3-Buten-2-ol, 2-methyl- (CA... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.02 0.23 ug/L 100357 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 78 2 Butenol, methyl- 86 C5H10O 060766-00-9 72 3 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 64 4 3-Buten-2-ol, 2-methyl-_____________ 86 C5H10O 000115-18-4 64 Abundance Scan 144 (5.018 min): 00472A.D (-) m/z 71.10 100.00% 43 TJI

5000 39 55 59 — TPT ■ ■ i ' 1 1 ' i ' ■ ■ 4.60 4.80 5.00 5.20 5.40 mlz~> 0b 5 llL , 511 ----- r ‘ " r ' " i ■ " • i ■' ■' i ” '11 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 , 67 i . 84 TPPP m/ z 43.10 85.14% Abundance #4088:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 7h

5000 1-- A । ।.. r P i ■> 59 4.60 4.80 5.00 5.20 5.40 m/z 41.10 71.31% 53 n r | n r ,| i i 11 ] > । i i । i > . i|-n epmmTPmmTMTTR . | . I I I | . TTHH ’-’— I r.-nfr.TTpin 85- 67 0 | '1| /z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4093: Butenol, methyl- 43 71 —4.604 4.80 5.00 5.20 5.40 A A _A

5000 59 m/z 69.10 43.85% 27 15 31 53 ob'1" i" " "‘T ■111 ■b' l11 67 —Tp — -FH 86 mlz~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #9384: 2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... 7h 4.60 4.80 5.00 5.20 5.40 43 m/ Z 59.10 34.43%

5000 27 31 53 0b piny 1.. . T 37 A .M m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

00472A.D HP020702.M Thu Feb 21 09:57:54 2002 Page 6

NYC-WTC_000052280

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NYC-WTC_000052280Source: NYC Law Department, mirrored locally

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