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GCMS results for sample AE00329, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00329 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051485–000051499

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00329.D Vial: 3 Acq On : 11 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rW 26020 38578 0.35% 0.064% 2 4.629 107 110 123 rVB2 12227 27086 0.24% 0.045% 3 4.858 123 130 141 rBV3 12113 42616 0.38% 0.071% 4 5.006 141 143 149 rVB2 20893 40707 0.37% 0.068% 5 5.885 217 220 247 rBV 687863 1467876 13.21% 2.450%

6 7.472 357 359 367 rBV 6431 22696 0.20% 0.038% 7 9.550 539 541 547 rBV2 15513 38463 0.35% 0.064% 8 9.641 547 549 551 rW 16574 30589 0.28% 0.051% 9 9.721 551 556 561 rW 2965398 6108053 54.96% 10.193% 10 9.847 561 567 577 rVB 16193 48682 0.44% 0.081%

11 13.192 855 860 865 rBV 4553699 8686074 78.15% 14.495% 12 18.341 1305 1311 1315 rBV 5198388 9828733 88.43% 16.402% 13 22.280 1651 1656 1661 rBV 37996 73628 0.66% 0.123% 14 22.645 1681 1688 1693 rBV 4975516 11036888 99.30% 18.418% 15 22.771 1695 1699 1715 rVB 62759 171046 1.54% 0.285%

16 24.849 1877 1881 1887 rVB 13560 28058 0.25% 0.047% 17 27.726 2129 2133 2139 rW 817603 1422422 12.80% 2.374% 18 30.500 2369 2376 2381 rBV 4488675 11114265 100.00% 18.547% 19 31.105 2425 2429 2439 rVB4 17010 60122 0.54% 0.100% 20 34.416 2713 2719 2749 rW 3730637 9637630 86.71% 16.083%

Sum of corrected areas: 59924212

00329.D SCAN508.M Mon Jan 14 10:46:46 2002 Page 1

NYC-WTC_000051489

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NYC-WTC_000051489Source: NYC Law Department, mirrored locally

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