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GCMS results for sample AE00321, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00321 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051394–000051407

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00321.D Vial: 2 Acq On : 11 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.614 19 21 25 rBV 36954 53867 0.46% 0.082% 2 4.630 107 110 117 rVB2 20454 37581 0.32% 0.057% 3 4.847 123 129 137 rBV2 18668 58750 0.50% 0.090% 4 5.018 141 144 14 9 rW 37895 65385 0.56% 0.100% 5 5.714 201 205 209 rBV2 18137 28156 0.24% 0.043%

6 5.886 217 220 245 rVB 994101 1859506 15.94% 2.840% 7 9.550 539 541 54 5 rW 11200 25729 0.22% 0.039% 8 9.642 545 54 9 551 rW 13797 29040 0.25% 0.044% 9 9.710 551 555 561 rW 3614109 7056849 60.50% 10.779% 10 9.847 561 567 577 rW 18366 61291 0.53% 0.094%

11 13.192 855 860 865 rBV 5278838 9996305 85.70% 15.269% 12 18.341 1305 1311 1315 rBV 5560608 10885261 93.32% 16.627% 13 22.280 1653 1656 1661 rBV 40154 71755 0.62% 0.110% 14 22.646 1681 1688 1693 rBV2 5206700 11664033 100.00% 17.816% 15 22.771 1695 1699 1717 rVB 60632 171445 1.47% 0.262%

16 24.849 1877 1881 1887 rVB 21431 39388 0.34% 0.060% 17 27.726 2129 2133 2139 rVB 821496 1436841 12.32% 2.195% 18 30.500 2369 2376 2381 rBV 4741400 11555916 99.07% 17.651% 19 31.105 2425 2429 2441 rW 17659 63788 0.55% 0.097% 20 34.416 2713 2719 2745 rBV 3941437 10307921 88.37% 15.745%

Sum of corrected areas: 65468807

00321.D SCAN508.M Mon Jan 14 10:46:42 2002 Page 1

NYC-WTC_000051398

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NYC-WTC_000051398Source: NYC Law Department, mirrored locally

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