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GCMS analysis results for sample AE00100, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050354–000050369

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00100.D Vial: 3 Acq On : 23 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rBV 40338 60506 0.50% 0.092% 2 4.241 71 76 83 rW3 42851 89259 0.74% 0.136% 3 4.367 83 87 91 rVB2 46500 83755 0.69% 0.128% 4 4.835 123 128 139 rBV 29000 75799 0.63% 0.116% 5 5.897 217 221 243 rVB 331740 736773 6.08% 1.123%

6 9.447 527 532 539 rVB2 16204 50302 0.41% 0.077% 7 9.550 539 541 545 rBV 16287 41950 0.35% 0.064% 8 9.710 551 555 561 rW 3584519 7300588 60.21% 11.125% 9 12.541 799 803 807 rVB 27944 43050 0.36% 0.066% 10 13.192 855 860 865 rBV 5300288 10436237 86.07% 15.903% • 11 18.341 1305 1311 1315 rBV 5587897 11322365 93.38% 17.254% 12 21.184 1557 1560 1569 rW2 15857 43113 0.36% 0.066% 13 22.280 1651 1656 1661 rBV 49277 91894 0.76% 0.140% 14 22.645 1681 1688 1693 rBV 5431377 12125684 100.00% 18.478% 15 22.771 1695 1699 1707 rVB 61761 158720 1.31% 0.242% 16 24.849 1877 1881 1887 rW 94791 171549 1.41% 0.261% 17 26.013 1977 1983 1989 rW 280783 549206 4.53% 0.837% 18 27.726 2127 2133 2139 rW 831573 1470451 12.13% 2.241% 19 30.500 2369 2376 2381 rBV 4540001 11253738 92.81% 17.149% 20 34.416 2713 2719 2749 rBV 3520752 9518572 78.50% 14.505%

Sum of corrected areas: 65623511

00100.D SCAN508.M Thu Jan 24 09:57:09 2002 Page 1

NYC-WTC_000050358

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