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GCMS results for sample AE00314, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051364–000051379

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.488 5 10 13 rBV 29688 45959 0.38% 0.069% 2 3.614 17 21 25 rBV 30405 50274 0.41% 0.076% 3 4.630 103 110 119 rBV5 19464 47666 0.39% 0.072% 4 4.835 125 128 137 rBV3 25893 77319 0.64% 0.116% 5 5.006 141 143 149 rVB 31250 56647 0.47% 0.085%

6 5.885 217 220 229 rBV 868875 1655653 13.66% 2.494% 7 9.573 537 543 547 rW2 12400 37950 0.31% 0.057% 8 9.710 551 555 561 rW 3782244 7088714 58.48% 10.679% 9 9.847 565 567 577 rW 15601 50621 0.42% 0.076% 10 12.542 799 803 807 rVB 25023 41223 0.34% 0.062%

11 13.192 855 860 865 rBV 5437175 10176027 83.95% 15.331% 12 18.341 1305 1311 1315 rBV 5579472 11210979 92.49% 16.890% 13 22.280 1651 1656 1661 rW 48992 88378 0.73% 0.133% 14 22.645 1681 1688 1693 rW2 5219364 12121247 100.00% 18.261% 15 22.771 1695 1699 1711 rVB 71554 181744 1.50% 0.274%

16 24.849 1877 1881 1889 rVB 20268 42118 0.35% 0.063% 17 27.726 2129 2133 2137 rBV 885155 1554813 12.83% 2.342% 18 30.489 2369 2375 2381 rBV 4606141 11627466 95.93% 17.517% 19 31.105 2425 2429 2437 rVB3 7759 30234 0.25% 0.046% 20 34.416 2713 2719 2755 rBV 3884980 10191983 84.08% 15.355%

Sum of corrected areas: 66377015

30314.D SCAN508.M Tue Jan 15 08:47:50 2002 Page 1

NYC-WTC_000051368

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NYC-WTC_000051368Source: NYC Law Department, mirrored locally

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