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GCMS analysis results for sample AD31585, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31585 including unknown compounds and surrogate recovery data.

NYC-WTC_000049902–000049915

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000049906
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN17\31585.D Vial: 1 Acq On : 17 Jan 2002 2:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.465 5 8 11 rVB 17186 25377 0.27% 0.050% 2 3.590 17 19 25 rBV 22722 42132 0.44% 0.083% 3 4.230 71 75 83 rW3 5351 18774 0.20% 0.037% 4 4.355 83 86 91 rVB 11300 19050 0.20% 0.038% 5 4.618 107 109 117 rVB3 13944 30530 0.32% 0.060% 6 4.846 125 129 139 rBV6 14891 50415 0.53% 0.100% 7 4.995 139 142 149 rVB3 10503 28209 0.30% 0.056% 8 5.885 215 220 251 rVB 529435 1356041 14.28% 2.682% 9 9.710 551 555 563 rBV 2588541 5457493 57.47% 10.795% 10 13.192 855 860 865 rBV 4115782 7697049 81.05% 15.226% 11 18.341 1305 1311 1315 rBV 4482886 8555786 90.09% 16.924% 12 21.184 1553 1560 1571 rW4 4516 19988 0.21% 0.040% 13 22.280 1653 1656 1661 rBV2 33996 63179 0.67% 0.125% 14 22.634 1681 1687 1693 rBV2 4285624 9496447 100.00% 18.785% 15 22.771 1695 1699 1703 rVB 45976 107417 1.13% 0.212% 16 24.849 1877 1881 1887 rVB 60936 108888 1.15% 0.215% 17 27.726 2127 2133 2139 rW 685497 1205415 12.69% 2.384% 18 30.489 2369 2375 2381 rBV2 3825405 8866040 93.36% 17.538% 19 33.400 2625 2630 2635 rBV2 21988 47753 0.50% 0.094% 20 34.416 2713 2719 2751 rBV 2876202 7357536 77.48% 14.554%

Sum of corrected areas: 50553519

31585.D SCAN508.M Tue Jan 22 08:36:50 2002 Page 1

NYC-WTC_000049906

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NYC-WTC_000049906Source: NYC Law Department, mirrored locally

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