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GCMS analysis results for sample AD31631, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31631 including unknown compounds and surrogate recovery data.

NYC-WTC_000049916–000049928

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000049920
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31631.D Vial: 3 Acq On : 17 Jan 2002 11:52 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.591 15 19 25 rBV 24532 42895 0.42% 0.078% 2 4.253 73 77 81 rBV3 5297 17295 0.17% 0.032% 3 4.356 81 86 91 rVB 13804 25703 0.25% 0.047% 4 4.618 107 109 113 rW3 11776 22595 0.22% 0.041% 5 4.846 125 129 139 rBV4 15954 55646 0.55% 0.102% 6 4.995 139 142 151 rVB4 11385 31458 0.31% 0.058% 7 5.885 217 220 243 rBV 545341 1378700 13.58% 2.521% 8 9.710 551 555 563 rBV 2665454 5853841 57.66% 10.704% 9 12.541 799 803 809 rBV 7820 18223 0.18% 0.033% 10 13.192 855 860 865 rBV 4348535 8424022 82.98% 15.403% 11 13.386 873 877 893 rVB3 7493 27491 0.27% 0.050% 12 18.341 1305 1311 1315 rBV 4775684 9260214 91.22% 16.932% 13 22.280 1651 1656 1661 rBV 34669 66901 0.66% 0.122% 14 22.634 1681 1687 1693 rBV2 4604849 10151494 100.00% 18.562% 15 22.771 1695 1699 1707 rVB 50986 136519 1.34% 0.250% 16 24.849 1877 1881 1889 rW 61804 108881 1.07% 0.199% 17 27.726 2127 2133 2139 rW 742095 1307438 12.88% 2.391% 18 29.678 2301 2304 2311 rBV4 5733 16579 0.16% 0.030% 19 30.489 2369 2375 2381 rBV2 4221479 9730484 95.85% 17.792% 20 34.416 2713 2719 2745 rBV 3114576 8013283 78.94% 14.652%

Sum of corrected areas: 54689662

31631.D SCAN508.M Tue Jan 22 08:36:54 2002 Page 1

NYC-WTC_000049920

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NYC-WTC_000049920Source: NYC Law Department, mirrored locally

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