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GCMS results for sample AE00315, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00315 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051380–000051393

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN14\00315.D Vial: 4 Acq On : 14 Jan 2002 12:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.614 19 21 29 rW 19059 36406 0.28% 0.053% 2 4.630 101 110 119 rBV5 13804 31017 0.24% 0.045% 3 4.847 125 129 135 rBV3 15291 44610 0.34% 0.065% 4 5.006 141 143 149 rVB2 24627 46395 0.36% 0.067% 5 5.714 201 205 209 rBV2 15367 31310 0.24% 0.045%

6 5.885 217 220 239 rBV 646339 1333590 10.27% 1.935% 7 9.710 551 555 561 rW 3683158 7306303 56.25% 10.599% 8 9.847 561 567 577 rVB2 13604 45907 0.35% 0.067% 9 13.192 855 860 865 rBV 5495695 10448902 80.45% 15.158% 10 18.341 1305 1311 1315 rBV 6020240 11748779 90.46% 17.043%

11 22.280 1653 1656 1659 rBV2 52689 94607 0.73% 0.137% 12 22.645 1681 1688 1693 rW2 5730143 12988332 100.00% 18.842% 13 22.771 1693 1699 1719 rVB 72870 220865 1.70% 0.320% 14 24.849 1877 1881 1887 rW 16521 30966 0.24% 0.045% 15 27.726 2127 2133 2137 rBV 874999 1530019 11.78% 2.220%

16 29.678 2299 2304 2311 rVB2 9529 33954 0.26% 0.049% 17 30.500 2369 2376 2381 rBV 5051684 12400928 95.48% 17.989% 18 31.105 2425 2429 2439 rVB4 10534 40749 0.31% 0.059% 19 33.400 2625 2630 2639 rBV2 27685 74187 0.57% 0.108% 20 34.416 2713 2719 2745 rBV 3921242 10446731 80.43% 15.155%

Sum of corrected areas: 68934557

30315.D SCAN508 .M Tue Jan 15 08:47:54 2002 Page 1

NYC-WTC_000051384

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NYC-WTC_000051384Source: NYC Law Department, mirrored locally

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