GCMS results for sample AE00469, Jan 24 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00469.D Vial: 8 Acq On : 11 Jan 2002 7 : 55 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.614 17 21 25 rBV 28419 45237 0.37% 0.068% 2 4.630 103 110 117 rVB4 20173 47739 0.39% 0.072% 3 4.847 125 129 141 rBV3 19161 59324 0.49% 0.089% 4 5.006 141 143 14 7 rW 21766 40068 0.33% 0.060% 5 5.886 215 220 243 rBV 867148 1680935 13.87% 2.532%

6 9.710 551 555 561 rW 3862859 7757521 64.02% 11.683% 7 9.847 561 567 575 rVB 14219 38946 0.32% 0.059% 8 13.192 855 860 865 rBV 5746168 11005677 90.82% 16.575% 9 18.341 1305 1311 1315 rBV 5896942 11719549 96.71% 17.650% 10 19.997 1451 1456 1461 rVB2 20161 40998 0.34% 0.062%

11 22.280 1653 1656 1659 rW2 46512 78092 0.64% 0.118% 12 22.646 1681 1688 1693 rW 5382082 12118001 100.00% 18.250% 13 22.771 1695 1699 1713 rVB 64892 184777 1.52% 0.278% 14 24.849 1877 1881 1885 rW 40058 72541 0.60% 0.109% 15 27.726 2129 2133 2139 rBV 611475 1075284 8.87% 1.619%

16 29.244 2261 2266 2275 rVB2 18606 41890 0.35% 0.063% 17 30.500 2369 2376 2381 rBV 4435217 11069305 91.35% 16.671% 18 31.105 2417 2429 2441 rBV5 20197 94683 0.78% 0.143% 19 33.503 2635 2639 2649 rVB 22812 99669 0.82% 0.150% 20 34.416 2713 2719 2745 rBV 3552773 9130321 75.35% 13.750%

Sum of corrected areas: 66400557

00469.D SCAN508.M Mon Jan 14 10:47:10 2002 Page 1

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