GCMS results for sample AE00462, Jan 24 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\5973N\02JANll\00462.D Vial: 4 Acq On : 11 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.613 19 21 25 rBV 35469 49965 0.41% 0.074% 2 3.921 43 48 53 rVB 15244 23809 0.19% 0.035% 3 4.629 107 110 119 rVB 16056 33980 0.28% 0.050% 4 4.846 125 129 141 rBV2 17778 57438 0.47% 0.085% 5 5.006 141 143 149 rBV 74017 127017 1.04% 0.188%

6 5.714 201 205 209 rVB 47753 83354 0.68% 0.123% 7 5.885 217 220 241 rW 815122 1568583 12.82% 2.321% 8 9.561 539 542 54 7 rW2 9207 26370 0.22% 0.039% 9 9.710 551 555 561 rW 3872395 7453610 60.93% 11.029% 10 9.847 561 567 575 rW2 13993 50915 0.42% 0.075%

11 12.541 799 803 807 rVB 16131 24937 0.20% 0.037% 12 13.192 855 860 865 rBV 5531235 10703502 87.50% 15.837% 13 18.341 1305 1311 1315 rBV 5847158 11497589 93.99% 17.012% 14 19.973 1445 1454 1459 rW3 4837 23551 0.19% 0.035% 15 22.280 1651 1656 1661 rBV 48849 89182 0.73% 0.132%

16 22.645 1681 1688 1693 rBV 5508383 12232880 100.00% 18.100% 17 22.771 1695 1699 1715 rVB 69205 188064 1.54% 0.278% 18 27.726 2129 2133 2139 rBV 839709 1502991 12.29% 2.224% 19 30.500 2369 2376 2381 rBV 4732135 11652154 95.25% 17.241% 20 34.416 2713 2719 2747 rBV 3973560 10194806 83.34% 15.084%

Sum of corrected areas: 67584697

30462.D SCAN508.M Mon Jan 14 10:46:50 2002 Page 1

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