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GCMS analysis results for sample AE00839, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.

NYC-WTC_000052088–000052107

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052092
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00839.D Vial: 3 Acq On : 31 Jan 2002 4:21 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.613 17 21 25 rBV 32391 47344 0.27% 0.049% 2 5.063 145 148 161 rVB 70107 152195 0.86% 0.159% 3 5.920 221 223 229 rBV 97372 221711 1.26% 0.232% 4 6.000 229 230 247 rVB 333766 904192 5.13% 0.944% 5 9.710 551 555 561 rBV 5721171 11005752 62.50% 11.496%

6 11.502 709 712 719 rVB 32229 61465 0.35% 0.064% 7 11.776 731 736 747 rVB6 8754 51363 0.29% 0.054% 8 12.541 801 803 811 rW3 19853 69093 0.39% 0.072% 9 12.735 817 820 825 rW2 29347 56517 0.32% 0.059% 10 13.192 855 860 865 rBV 7809398 15824276 89.86% 16.529%

11 13.409 873 879 885 rW2 163180 323201 1.84% 0.338% 12 15.190 1031 1035 1043 rW 37336 68565 0.39% 0.072% 13 18.341 1305 1311 1315 rBV 8105610 16724110 94.97% 17.469% 14 18.433 1315 1319 1329 rVB 31846 109893 0.62% 0.115% 15 22.280 1651 1656 1661 rBV2 77102 142151 0.81% 0.148%

16 22.645 1681 1688 1693 rBV2 7421403 17609420 100.00% 18.393% 17 22.771 1695 1699 1717 rVB 106875 367718 2.09% 0.384% 18 27.726 2129 2133 2137 rBV 1084074 2053937 11.66% 2.145% 19 30.500 2369 2376 2381 rBV 6357053 16090155 91.37% 16.807% 20 34.416 2713 2719 2755 rBV 4909074 13854242 78.68% 14.471%

Sum of corrected areas: 95737300

00839.D SCAN508.M Fri Feb 01 09:19:13 2002 Page 1

NYC-WTC_000052092

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NYC-WTC_000052092Source: NYC Law Department, mirrored locally

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