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GCMS analysis results for sample AE00838, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052187–000052204

Folder label: “GCMS X 1/11/02 A 1/31/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508 .M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 6.023 229 232 257 rVB 160861 515800 3.56% 0.609% 2 6.685 287 290 321 rBV3 100936 1457282 10.06% 1.720% 3 9.710 551 555 561 rBV 4496577 8730675 60.29% 10.306% 4 11.229 671 688 699 rVB3 78219 666622 4.60% 0.787% 5 13.192 855 860 865 rBV 6481207 12404241 85.66% 14.642%

6 16.857 1177 1181 1185 rBV 189953 349764 2.42% 0.413% 7 18.341 1305 1311 1315 rBV 6649282 13502969 93.25% 15.939% 8 18.433 1315 1319 1325 rW 473837 835359 5.77% 0.986% 9 19.917 1445 1449 1453 rBV 151745 278644 1.92% 0.329% 10 21.333 1567 1573 1577 rBV 132508 251890 1.74% 0.297%

11 22.280 1653 1656 1669 rVB3 86170 297073 2.05% 0.351% 12 22.646 1681 1688 1693 rBV 6293554 14480216 100.00% 17.093% 13 22.771 1695 1699 1711 rVB3 95133 339091 2.34% 0.400% 14 24.723 1865 1870 1877 rBV 140145 322072 2.22% 0.380% 15 26.014 1977 1983 1989 rBV 632820 1260704 8.71% 1.488%

16 27.726 2127 2133 2137 rBV 997591 1853154 12.80% 2.187% 17 30.489 2369 2375 2381 rBV2 5403377 13892019 95.94% 16.398% 18 34.416 2713 2719 2751 rBV 4257600 11563258 79.86% 13.649% 19 35.912 2845 2850 2875 rBV2 225108 1011275 6.98% 1.194% 20 36.289 2875 2883 2901 rBV2 99858 703734 4.86% 0.831%

Sum of corrected areas: 84715842

00831.D SCAN508.M Fri Feb 01 09:18:42 2002 Page 1

NYC-WTC_000052189

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NYC-WTC_000052189Source: NYC Law Department, mirrored locally

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