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GCMS analysis results for sample AE00830, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.

NYC-WTC_000052047–000052068

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052051
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.613 17 21 25 rBV 32015 53899 0.35% 0.066% 2 4.915 129 135 141 rVB3 11246 35869 0.23% 0.044% 3 5.018 141 144 149 rBV 56880 102231 0.65% 0.124% 4 5.714 201 205 209 rVB2 37128 61886 0.40% 0.075% 5 5.931 221 224 233 rBV 89229 239020 1.53% 0.291%

6 6.068 233 236 253 rW 36054 116165 0.74% 0.141% 7 9.584 539 544 551 rBV5 9310 34118 0.22% 0.042% 8 9.710 551 555 561 rW 5059139 9387335 60.09% 11.421% 9 9.881 567 570 581 rVB3 10833 49331 0.32% 0.060% 10 13.192 855 860 865 rBV 7041968 13672526 87.52% 16.635%

11 13.409 871 879 883 rVB2 17679 65630 0.42% 0.080% 12 16.549 1149 1154 1157 rVB2 19921 37254 0.24% 0.045% 13 18.341 1305 1311 1315 rBV 7198943 14816247 94.85% 18.026% 14 22.280 1651 1656 1661 rBV 67376 125891 0.81% 0.153% 15 22.645 1681 1688 1693 rBV 6679399 15621370 100.00% 19.006%

16 22.771 1695 1699 1729 rVB 92805 352491 2.26% 0.429% 17 26.002 1979 1982 1987 rBV 21422 48752 0.31% 0.059% 18 27.726 2129 2133 2137 rBV 959800 1852839 11.86% 2.254% 19 30.500 2369 2376 2381 rBV 5302319 13862890 88.74% 16.866% 20 34.416 2713 2719 2751 rBV 4278309 11657062 74.62% 14.183%

Sum of corrected areas: 82192806

00830.D SCAN508.M Fri Feb 01 09:18:30 2002 Page 1

NYC-WTC_000052051

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NYC-WTC_000052051Source: NYC Law Department, mirrored locally

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