GCMS instrument data file SCAN508, Jan 31 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\O2 JAN31\00845.D Vial: 6 Acq On : 31 Jan 2002 6:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.931 221 224 231 rBV 69600 165017 1.00% 0.182% 2 6.034 231 233 247 rW 100103 264334 1.59% 0.291% 3 6.639 283 286 321 rBV3 188524 2478959 14.95% 2.731% 4 9.710 551 555 563 rBV 4839920 9556526 57.63% 10.529% 5 11.263 673 691 697 rBV4 88501 773757 4.67% 0.852%

6 12.736 817 820 825 rBV 76217 148031 0.89% 0.163% 7 13.067 841 849 855 rBV8 41818 219705 1.32% 0.242% 8 13.192 855 860 865 rBV 7051871 13820154 83.34% 15.226% 9 13.409 875 879 885 rVB 566894 982224 5.92% 1.082% 10 14.711 987 993 1001 rVB2 43665 147135 0.89% 0.162%

11 15.190 1031 1035 1045 rVB 250062 465670 2.81% 0.513% 12 16.857 1177 1181 1187 rBV 128236 234961 1.42% 0.259% 13 18.341 1305 1311 1315 rBV 7621084 15524771 93.62% 17.104% 14 18.433 1315 1319 1323 rW 80199 166609 1.00% 0.184% 15 22.645 1681 1688 1693 rBV2 6957975 16582535 100.00% 18.270%

16 22.771 1695 1699 1715 rVB 101226 317627 1.92% 0.350% 17 27.726 2127 2133 2137 rBV 889796 1694123 10.22% 1.866% 18 30.489 2369 2375 2381 rBV2 5781745 14814381 89.34% 16.322% 19 31.105 2423 2429 2441 rW 58928 219927 1.33% 0.242% 20 34.416 2713 2719 2753 rBV 4379420 12189138 73.51% 13.429%

Sum of corrected areas: 90765584

00845.D SCAN508.M Fri Feb 01 09:19:34 2002 Page 1

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