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GCMS analysis results for sample AD31671, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.

NYC-WTC_000050024–000050038

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000050028
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\O2JAN17\31671.D Vial: 6 Acq On : 17 Jan 2002 6:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rBV 35727 53437 0.45% 0.083% 2 3.978 49 53 59 rW 16632 29263 0.25% 0.046% 3 4.241 71 76 83 rW2 29070 66727 0.57% 0.104% 4 4.618 107 109 123 rW 22386 50661 0.43% 0.079% 5 4.823 123 127 141 rW3 43122 109301 0.93% 0.170% 6 5.885 217 220 247 rVB 870550 1889047 16.05% 2.938% 7 9.710 551 555 561 rBV 3490632 6652327 56.51% 10.345% 8 12.541 799 803 809 rW 33006 55147 0.47% 0.086% 9 13.192 855 860 865 rBV 4968831 9489114 80.61% 14.757% 10 18.341 1305 1311 1315 rBV 5378571 10597991 90.03% 16.482% 11 21.332 1569 1573 1577 rW 15256 24968 0.21% 0.039% 12 22.280 1651 1656 1661 rW 43763 83048 0.71% 0.129% 13 22.645 1681 1688 1693 rBV2 5202262 11771284 100.00% 18.306% 14 22.771 1695 1699 1707 rVB 66066 175698 1.49% 0.273% 15 24.849 1877 1881 1887 rBV 126849 228145 1.94% 0.355% 16 27.726 2127 2133 2139 rBV 795854 1412375 12.00% 2.196% 17 29.678 2301 2304 2315 rVB2 8606 26702 0.23% 0.042% 18 30.500 2369 2376 2381 rBV 4710941 11552749 98.14% 17.966% 19 31.105 2419 2429 2445 rVB3 21128 102204 0.87% 0.159% 20 34.416 2713 2719 2745 rBV 3829858 9932151 84.38% 15.446%

Sum of corrected areas: 64302339

1671.D SCAN508.M Tue Jan 22 08:37:26 2002 Page 1

NYC-WTC_000050028

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NYC-WTC_000050028Source: NYC Law Department, mirrored locally

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