GCMS analysis results for sample AE00615, Feb 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN29\00615.D Vial: 4 Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rBV 36653 63318 0.39% 0.073% 2 4.241 73 76 83 rBV3 43690 95632 0.59% 0.111% 3 4.630 103 110 117 rVB6 ' 18098 58756 0.36% 0.068% 4 4.846 123 129 137 rBV2 24122 77171 0.48% 0.089% 5 5.006 141 143 151 rVB 34115 65318 0.40% 0.076%

6 5.714 203 205 209 rVB 19361 34583 0.21% 0.040% 7 5.885 217 220 241 rBV 832463 1836502 11.35% 2.123% 8 9.721 551 556 561 rBV 4639295 9315470 57.60% 10.770% 9 12.541 799 803 807 rW 55350 91245 0.56% 0.105% 10 13.192 855 860 865 rBV 6732944 13343186 82.50% 15.427%

11 18.341 1305 1311 1315 rBV 7540038 14842650 91.77% 17.161% 12 22.280 1653 1656 1661 rBV2 62655- 128677 0.80% 0.149% 13 22.645 1681 1688 1693 rBV2 7182710 16173915 100.00% 18.700% 14 22.771 1695 1699 1723 rVB 98367 374724 2.32% 0.433% 15 24.849 1877 1881 1887 rW 89210 167452 1.04% 0.194%

16 27.726 2127 2133 2139 rBV 1132460 2050861 12.68% 2.371% 17 29.690 2299 2305 2315 rBV3 9456 36029 0.22% 0.042% 18 30.500 2369 2376 2381 rBV 6092414 15127263 93.53% 17.490% 19 31.105 2421 2429 2435 rBV5 10930 40978 0.25% 0.047% 20 34.416 2713 2719 2741 rBV 4734220 12567196 77.70% 14.530%

Sum of corrected areas: 86490926

0615.D SCAN508.M Wed Jan 30 09:02:19 2002 Page 1

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