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GCMS analysis results for sample AE00698, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050397–000050410

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00698.D Vial: 6 Acq On : 23 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.499 9 11 15 rVB 22765 31616 0.26% 0.050% 2 3.614 19 21 25 rBV 26862 38881 0.32% 0.061% 3 5.908 219 222 229 rBV 81191 191068 1.59% 0.301% 4 6.011 229 231 239 rVB 12915 24160 0.20% 0.038% 5 7.472 357 359 363 rBV 8080 21623 0.18% 0.034% 6 9.710 551 555 561 rW 3768230 7134183 59.55% 11.246% 7 9.847 561 567 579 rVB 13291 42219 0.35% 0.067% 8 13.192 855 860 865 rBV 5253683 10118451 84.46% 15.950% 9 13.375 873 876 883 rBV2 8667 23550 0.20% 0.037% 10 16.549 1149 1154 1159 rVB2 10611 19494 0.16% 0.031% 11 18.341 1305 1311 1315 rBV 5419263 11085256 92.53% 17.474% 12 22.280 1651 1656 1661 rBV2 45254 83979 0.70% 0.132% 13 22.645 1681 1688 1693 rBV2 5175504 11980597 100.00% 18.886% 14 22.771 1695 1699 1711 rVB 61847 175526 1.47% 0.277% 15 24.712 1865 1869 1875 rBV 18836 32541 0.27% 0.051% 16 27.052 2069 2074 2083 rVB 45732 84535 0.71% 0.133% 17 27.726 2129 2133 2137 rBV 808397 1413635 11.80% 2.228% 18 30.489 2369 2375 2381 rBV2 4459389 11041172 92.16% 17.405% 19 33.400 2625 2630 2663 rBV 116749 458777 3.83% 0.723% 20 34.416 2713 2719 2743 rBV 3425443 9435516 78.76% 14.874%

Sum of corrected areas: 63436779

00698.D SCAN508.M Thu Jan 24 09:57:22 2002 Page 1

NYC-WTC_000050401

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