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GCMS analysis results for sample AE00839, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00839 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050421–000050431

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050425
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00839.D Vial: 8 Acq On : 23 Jan 2002 8:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.488 5 10 15 rVB 16254 25523 0.23% 0.043% 2 3.602 19 20 25 rVB 23102 39120 0.35% 0.065% 3 3.922 45 48 53 rBV 10251 17159 0.15% 0.029% 4 4.241 71 76 85 rVB4 10207 28340 0.25% 0.047% 5 6.011 227 231 235 rBV 10292 16358 0.15% 0.027% 6 6.079 235 237 247 rVB2 6093 21772 0.19% 0.036% 7 9.562 539 542 547 rBV3 8566 21293 0.19% 0.036% 8 9.642 547 549 551 rW 9538 17457 0.16% 0.029% 9 9.710 551 555 561 rW 3521608 6746973 60.34% 11.283% 10 9.847 561 567 581 rVB 12433 43149 0.39% 0.072% 11 13.192 855 860 865 rBV 4922463 9585457 85.73% 16.030% 12 18.341 1305 1311 1315 rBV 5243905 10452860 93.48% 17.480% 13 22.280 1653 1656 1661 rW2 40748 74081 0.66% 0.124% 14 22.634 1681 1687 1693 rBV2 4929823 11181617 100.00% 18.699% 15 22.771 1695 1699 1705 rVB 60625 154548 1.38% 0.258% 16 24.849 1877 1881 1885 rVB 14464 26085 0.23% 0.044% 17 27.726 2127 2133 2139 rBV 675442 1174903 10.51% 1.965% 18 30.500 2369 2376 2381 rBV 4304492 10798754 96.58% 18.059% 19 31.094 2421 2428 2435 rVB3 5976 22081 0.20% 0.037% 20 34.416 2713 2719 2747 rBV 3420231 9350637 83.63% 15.637%

Sum of corrected areas: 59798167

00839.D SCAN508.M Thu Jan 24 09:57:28 2002 Page 1

NYC-WTC_000050425

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NYC-WTC_000050425Source: NYC Law Department, mirrored locally

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