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GCMS analysis results for sample AE00101, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050370–000050383

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00101.D Vial: 4 Acq On : 23 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rBV 41230 59872 0.50% 0.098% 2 4.241 71 76 83 rW2 26145 56896 0.48% 0.093% 3 4.367 83 87 91 rVB2 28271 46393 0.39% 0.076% 4 4.630 105 110 121 rVB5 13153 35332 0.30% 0.058% 5 4.846 125 129 141 rW2 13661 43205 0.36% 0.071% 6 5.006 141 143 147 rVB 13640 22418 0.19% 0.037% 7 5.920 221 223 235 rBV 44606 107455 0.90% 0.176% 8 9.710 551 555 561 rW 3334272 6564745 55.27% 10.773% 9 12.541 799 803 807 rVB 20804 34395 0.29% 0.056% 10 13.192 855 860 865 rBV 5009468 9477036 79.79% 15.552% 11 18.341 1305 1311 1315 rBV 5359673 10703457 90.11% 17.565% 12 22.280 1653 1656 1661 rBV2 44203 82393 0.69% 0.135% 13 22.645 1681 1688 1693 rBV2 5129192 11878023 100.00% 19.492% 14 22.771 1695 1699 1707 rVB 61421 160767 1.35% 0.264% 15 24.849 1877 1881 1889 rVB 92112 171062 1.44% 0.281% 16 26.013 1977 1983 1987 rBV 24143 49990 0.42% 0.082% 17 27.726 2129 2133 2139 rW 829786 1484113 12.49% 2.435% 18 30.489 2369 2375 2381 rBV 4293703 10887167 91.66% 17.866% 19 34.108 2689 2692 2697 rBV 12723 24930 0.21% 0.041% 20 34.416 2713 2719 2755 rBV 3293986 9048356 76.18% 14.848%

Sum of corrected areas: 60938005

00101.D SCAN508.M Thu Jan 24 09:57:13 2002 Page 1

NYC-WTC_000050374

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